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144282-37-1

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144282-37-1 Structure

144282-37-1 Structure
IdentificationBack Directory
[Name]

Carbamic acid, [(7S)-5-(phenylmethyl)-5-azaspiro[2.4]hept-7-yl]-, 1,1-dimethylethyl ester
[CAS]

144282-37-1
[Synonyms]

[(7S)-5-(Phenylmethyl)-5-azaspiro[2.4]hept-7-yl]carbamic
tert-butyl (S)-(5-benzyl-5-azaspiro[2.4]heptan-7-yl)carbamate
(S)-tert-Butyl (5-benzyl-5-azaspiro[2.4]heptan-7-yl)carbaMate
tert-butyl N-[(7S)-5-benzyl-5-azaspiro[2.4]heptan-7-yl]carbamate
[(7S)-5-(Phenylmethyl)-5-azaspiro[2.4]hept-7-yl]carbamic acid tert-butyl ester
Carbamic acid, [(7S)-5-(phenylmethyl)-5-azaspiro[2.4]hept-7-yl]-, 1,1-dimethylethyl ester
CarbaMic acid, N-[(7S)-5-(phenylMethyl)-5-azaspiro[2.4]hept-7-yl]-, 1,1-diMethylethyl ester
[EINECS(EC#)]

1806241-263-5
[Molecular Formula]

C18H26N2O2
[MDL Number]

MFCD17214772
[MOL File]

144282-37-1.mol
[Molecular Weight]

302.41
Chemical PropertiesBack Directory
[Boiling point ]

420.5±34.0 °C(Predicted)
[density ]

1.12
[storage temp. ]

Sealed in dry,2-8°C
[pka]

12.31±0.20(Predicted)
[Appearance]

White to off-white Solid
[Optical Rotation]

Consistent with structure
[InChI]

InChI=1S/C18H26N2O2/c1-17(2,3)22-16(21)19-15-12-20(13-18(15)9-10-18)11-14-7-5-4-6-8-14/h4-8,15H,9-13H2,1-3H3,(H,19,21)/t15-/m1/s1
[InChIKey]

UCBLMUMETZZNIZ-OAHLLOKOSA-N
[SMILES]

C(OC(C)(C)C)(=O)N[C@H]1C2(CC2)CN(CC2=CC=CC=C2)C1
Hazard InformationBack Directory
[Uses]

Used in pharmaceutical synthesis and scientific research experiments.
[Synthesis]

3.75 g of 5-benzyl-5-azaspiro[2.4]heptan-7-amine was added to the reaction flask, followed by 35 mL of ethanol, 3.75 g of triethylamine and 6.5 g of Boc2O.Stir the reaction at room temperature for 12-14 hours, concentrate, add ethyl acetate, and then use aqueous lemon solution, sodium bicarbonate solution, and saturatedWashed with brine, dried, concentrated and dried to give tert-Butyl (S)-(5-benzyl-5-azaspiro[2.4]heptan-7-yl)carbamate.The yield was 98.2%.
Carbamic acid, [(7S)-5-(phenylmethyl)-5-azaspiro[2.4]hept-7-yl]-, 1,1-dimethylethyl ester
Spectrum DetailBack Directory
[Spectrum Detail]

tert-Butyl (S)-(5-benzyl-5-azaspiro[2.4]heptan-7-yl)carbamate(144282-37-1)1HNMR
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