| Identification | Back Directory | [Name]
4-Chluoro-2-bromotoluene | [CAS]
1445684-99-0 | [Synonyms]
CarolGold
Palm-Glu-OtBu
Fmoc-D-Ala-Ala-OH
CarolGold (Lutein)
Magnolol & Honokiol
BOC-(D)-HIS(TRT)-AIB
CarolZea (Zeaxanthin)
Endoxifen (E-isomer )
Octa(OtBu)-D-Glu-OtBu
Boc-D-His(Trt)-Aib-OH
tBu-OOC-C18-CO-Glu-OtBu
Hydrolyzed silk protein
4-Chluoro-2-bromotoluene
CarolGold (Lutein) Powder
Octadecane(OtBu)-Glu-OtBu
Canthaxanthin Beadlet 10%
Nucleating agent NA-9930T
CarolGold (Lutein) EMulsion
Octadecane(OtBu)-D-Glu-OtBu
tBu-OOC-C14-CO-Glu(NHS)-OtBu
Fmoc-D-Lys(Palm-Glu-OtBu)-OH
Fmoc-Lys(Palm-D-Glu-OtBu)-OH
Canthaxanthin Beadlet 10% TAB
Fmoc-D-Lys(Palm-D-Glu-OtBu)-OH
2-(4-Phenoxyphenyl)ethylboroni
3-(2-Trimethylsiloxyphenyl)-1-
3-Pentafluorophenyl-1-propylbo
Tetrahydrothiophene-1,1-dioxid
Trans-4-Bromo-beta-styrylboron
Canthaxanthin Beadlet 10% CWS-S
Cefpodoxime Proxetil Impurity I
Cefpodoxime Proxetil Impurity J
CarolGold (Lutein) Oil Suspension
Boc-His(Trt)-Aib-Glu(OtBu)-Gly-OH
Boc-His(Trt)-Aib-Glu(OtBu)-Gly-OR
Boc-His(Trt)-Aib-Glu(OtBu)-Gly-NHS
Cefpodoxime Proxetil EP Impurity J
Boc-D-His(Trt)-Aib-Glu(OtBu)-Gly-OH
Boc-His(Trt)-Aib-D-Glu(OtBu)-Gly-OH
CarolZea (Zeaxanthin) Oil Suspension
Octa(OtBu)-D-Glu(ɑ-OtBu)-AEEA-AEEA-OH
Boc-D-His(Trt)-Aib-D-Glu(OtBu)-Gly-OH
Octadecane(OtBu)-Glu(AEEA-AEEA-NHS)-OtBu
3-[(2,2,2-TRIFLUOROETHYL)SULFANYL]ANILINE
4-Fluoro-5-methyl-biphenyl-3-carbaldehyde
Octadecane(OtBu)-D-Glu(ɑ-OtBu)-AEEA-AEEA-OH
Benzenamine, 3-[(2,2,2-trifluoroethyl)thio]-
Polypropylene Β-crystal nucleating agent TMB-5
1-(2-chlorophenyl)-ethane-1,2-bismethanesulfonate
TIANFU-CHEM CAS NO.000-00-0 4-Chluoro-2-bromotoluene
3,6-dibromo-9-(4-(naphthalen-2-yl)phenyl)-9H-carbazole | [EINECS(EC#)]
-0 | [Molecular Formula]
C8H8F3NS | [MDL Number]
MFCD21805732 | [MOL File]
1445684-99-0.mol | [Molecular Weight]
207.22 |
| Hazard Information | Back Directory | [Uses]
3-((2,2,2-trifluoroethyl)thio)aniline can be used as an intermediate in pharmaceutical research. | [Synthesis]
To
a
solution
of
3-aminobenzenethiol
(4.43
g,
35.4
mmol)
in
THF
(225
mL)
was
added
sodium
hydride
(1.77
g,
44.3
mmol)
at
0
°C
and
stirred
for
30
min.
Then,
2,2,2-trifluoroethyl
4-
methylbenzenesulfonate
(9.0
g,
35.4
mmol)
was
added
and
the
reaction
mixture
was
stirred
for
18
h.
The
reaction
mixture
was
quenched
with
water
(20
mL)
and
extracted
with
EtOAc
(2x50
mL).
The
combined
organic
extracts
were
washed
with
water,
dried
over
Na2SO4,
fdtered,
and
concentrated
under
reduced
pressure.
The
crude
residue
was
purified
by
flash
chromatography
through
a
Redi-Sep
pre-packed
silica
gel
column,
eluting
with
a
gradient
of
5
%
to
10
%
EtOAc
in
hexanes,
to
give
3-((2,2,2-
trifluoroethyl)thio)aniline
(5
g,
68
%
yield)
as
a
pale
brown
oil. |
|
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