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144691-35-0

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144691-35-0 Structure

144691-35-0 Structure

Identification	Back Directory
[Name] 1-(2-Hydroxy-3-iodo-4-phenoxyphenyl)ethanone
[CAS] 144691-35-0
[Synonyms] 1-(2-Hydroxy-3-iodo-4-phenoxyphenyl)ethanone Ethanone, 1-(2-hydroxy-3-iodo-4-phenoxyphenyl)-
[Molecular Formula] C14H11IO3
[MOL File] 144691-35-0.mol
[Molecular Weight] 354.14

Chemical Properties	Back Directory
[Melting point ] 116–118°C
[Boiling point ] 366.5±42.0 °C(Predicted)
[density ] 1.670±0.06 g/cm3(Predicted)
[pka] 8.04±0.15(Predicted)

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[Preparation] Preparation by thermal rearrangement of 4-acetyl- 3-hydroxy-2-phenyliodonio-phenolate (SM) in refluxing acetonitrile for 30 min (70%). SM was obtained by reaction of iodosobenzene diacetate with resacetophenone in methanol in the presence of potassium hydroxide at 0° for 30 min (40%, m.p. 81–85°).

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