| Identification | Back Directory | [Name]
BIS(4-BROMOPHENYL)AMINE | [CAS]
16292-17-4 | [Synonyms]
Bis(4-bromophenyL
Bis(p-bromophenyl)amine
BIS(4-BROMOPHENYL)AMINE
II (4-bromophenyl) amine
4,4'-DIBROMODIPHENYLAMINE
4,4'-Di(bromophenyl)amine
Double(4-BroMophenyl)aMine
Bis(4-bromophenyl)amine 97%
Bis(4-bromophenyl)amine >
N-phenyl-4,4μ-dibromoaniline
4-bromo-N-(4-bromophenyl)aniline
BenzenaMine,4-broMo-N-(4-broMophenyl)-
Bis(4-bromophenyl)amine, 99%, for synthesis
BIS(4-BROMOPHENYL)AMINE ISO 9001：2015 REACH
4,4μ-Dibromodiphenylamine, N-phenyl-4,4μ-dibromoaniline
Bis(4-bromophenyl)amine,4,4′-Dibromodiphenylamine, N-phenyl-4,4′-dibromoaniline | [EINECS(EC#)]
628-026-3 | [Molecular Formula]
C12H9Br2N | [MDL Number]
MFCD00225488 | [MOL File]
16292-17-4.mol | [Molecular Weight]
327.01 |
| Questions And Answer | Back Directory | [Synthesis]
Under nitrogen protection, 3.77 g of p-bromochlorobenzene, 6.01 g of anhydrous K3PO4, 0.15 g of anhydrous Cu(CH3CO2)2 and 0.19 g of proline were added to a 100 mL three-necked flask. Then, 2.53 g of p-bromoaniline and 10 mL of DMF were injected using a syringe. After reacting at 130 °C for 4 h, the reaction was stopped, filtered, and most of the solvent was evaporated. The residue was diluted with distilled water and adjusted to pH 2-3. The residue was then filtered under vacuum, the filter cake was washed with ethyl acetate, and the filtrate was dried over anhydrous sodium sulfate. The solution was then concentrated under reduced pressure, and the residue was recrystallized to obtain a pale yellow solid (yield 93%, purity 99%).  | [Uses]
Di(4-bromophenyl)amine is an amine organic compound and an important intermediate in the synthesis of pressure-sensitive dyes, pharmaceuticals, rubber, pesticides, and adhesive excipients. |
| Chemical Properties | Back Directory | [Melting point ]
106 °C | [Boiling point ]
380.5±27.0 °C(Predicted) | [density ]
1.740±0.06 g/cm3(Predicted) | [storage temp. ]
Keep in dark place,Inert atmosphere,Room temperature | [solubility ]
soluble in Methanol | [form ]
powder to crystal | [pka]
-0.55±0.40(Predicted) | [color ]
White to Almost white | [InChI]
InChI=1S/C12H9Br2N/c13-9-1-5-11(6-2-9)15-12-7-3-10(14)4-8-12/h1-8,15H | [InChIKey]
VKVHTZNHLOGHGP-UHFFFAOYSA-N | [SMILES]
C1(NC2=CC=C(Br)C=C2)=CC=C(Br)C=C1 |
|
| Company Name: |
Sunshine Optoelectronic Gold
|
| Telephone: |
027-027-87915283 15972929998 |
| Website: |
http://www.sunshine-oled.com |
| Company Name: |
J & K SCIENTIFIC LTD.
|
| Telephone: |
18210857532 18210857532 |
| Website: |
https://www.jkchemical.com |
| Company Name: |
Energy Chemical
|
| Telephone: |
400-0056266 |
| Website: |
www.energy-chemical.com |
| Company Name: |
Jia Xing Isenchem Co.,Ltd
|
| Telephone: |
0573-85285100 18627885956 |
| Website: |
https://www.chemicalbook.com/ShowSupplierProductsList14265/0_EN.htm |
|