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174063-87-7

174063-87-7 Structure

174063-87-7 Structure
IdentificationBack Directory
[Name]

1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene
[CAS]

174063-87-7
[Synonyms]

RM257
RM257?98%min
1,4-Bis[4-(3-acryloyloxypropoxy)benzoyloxy]-2-methylbenzene
1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenze
2-Methyl-1,4-phenylene-bis[4[3(acryloyloxy)propyloxy]benzoate]
2-Methyl-1,4-phenylene bis(4-(3-(acryloyloxy)propoxy)benzoate)
1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene
4-(3-Acryloyloxypropyloxy)-benzoesure 2-methyl-1, 4-phenylester
4-(3-Acryloyloxypropyloxy)benzoic acid 2-methyl-1,4-phenylene ester
4- (3-acryloyloxy-propoxy) benzoic acid 2-methyl-1,4-phenylene ester
RM257 4-(3-Acryloyloxypropyloxy)benzoic acid 2-methyl-1,4-phenylene ester
Benzoic acid, 4-[3-[(1-oxo-2-propenyl)oxy]propoxy]-,2-methyl-1,4-phenylene ester
Benzoic acid, 4-[3-[(1-oxo-2-propen-1-yl)oxy]propoxy]-, 1,1'-(2-methyl-1,4-phenylene) ester
[3-methyl-4-[4-(3-prop-2-enoyloxypropoxy)benzoyl]oxyphenyl] 4-(3-prop-2-enoyloxypropoxy)benzoate
1,4-Bis[4-(3-acryloyloxypropoxy)benzoyloxy]-2-methylbenzene (This product is only available in Japan.)
1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-Methylbenzene 4-(3-Acryloyloxypropyloxy)-benzoesure -2-Methyl-1, 4-phenylester
[EINECS(EC#)]

425-560-7
[Molecular Formula]

C33H32O10
[MDL Number]

MFCD09743681
[MOL File]

174063-87-7.mol
[Molecular Weight]

588.6
Chemical PropertiesBack Directory
[Boiling point ]

733.5±60.0 °C(Predicted)
[density ]

1.219
[vapor pressure ]

0.003Pa at 25℃
[storage temp. ]

Keep in dark place,Sealed in dry,Room Temperature
[Water Solubility ]

5.3μg/L at 20℃
[LogP]

5.3 at 40℃
Hazard InformationBack Directory
[Chemical Properties]

white powder
[Application]

1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene is one of numerous organic compounds composing American Elements's comprehensive catalog of life science products.
[Flammability and Explosibility]

Notclassified
[Synthesis]

The synthesis of 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene is as follows:Stirrer, was added methanesulfonyl chloride 5.00 g (43.6 mmol) and tetrahydrofuran 10mL the reactor having a thermometer and two dropping device. Ice-cold while each by dropping a tetrahydrofuran solution 30mL of formula tetrahydrofuran solution 60mL and triethylamine 5.25g of (I-3-1) represented by the compound 12.9g (44.1 mmol) of (51.9 mmol) from device (equation (solution of the compound represented by I-3-1)) :( triethylamine solution) = 2: were added dropwise simultaneously with one of the drip rate.After stirring for 1 hour while cooling with ice, it was added 4-dimethylaminopyridine 2.64 g (21.6 mmol) and 2- (4-hydroxyphenyl) ethanol 2.69 g (19.4 mmol).With ice-cooling was added dropwise triethylamine 5.25g (51.9 mmol).After stirring for 7 hours, the solvent was distilled off and treated added for liquid separation dichloromethane and 5% hydrochloric acid.After the organic layer was washed with brine neutralization, and purified by column chromatography (silica gel) and reprecipitated (dichloromethane / methanol) to give the compound 12.2g of formula (I-3).82% yield, had a purity of 99.63%.

174063-87-7.png

Spectrum DetailBack Directory
[Spectrum Detail]

1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene(174063-87-7)1HNMR
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