| Identification | Back Directory | [Name]
6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine | [CAS]
18184-75-3 | [Synonyms]
NSC 151664
2,3-Pyridinedicarboximide,N-benzyl
N-Benzyl- 2,3-pyridinedicarboximide
6-Benzylpyrrolo[3,4-b]pyridine-5,7-dione
6-Benzyl-6H-pyrrolo[3,4-b]pyridine- 5,7-dione
6-Benzyl-5H-pyrrolo[3,4-b]pyridine-5,7(6H)-dione
6-benzyl-5H,6H,7H-pyrrolo[3,4-b]pyridine-5,7-dione
6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridin
6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine
6-(Phenylmethyl)-5H-pyrrolo[3,4-b]pyridine-5,7(6H)-dione | [Molecular Formula]
C14H10N2O2 | [MDL Number]
MFCD02930145 | [MOL File]
18184-75-3.mol | [Molecular Weight]
238.24 |
| Chemical Properties | Back Directory | [Appearance]
Off-White Solid | [Melting point ]
154-156°C | [Boiling point ]
418.9±28.0 °C(Predicted) | [density ]
1.368±0.06 g/cm3(Predicted) | [storage temp. ]
Refrigerator | [solubility ]
DMSO (Slightly), Methanol (Slightly) | [form ]
Solid | [pka]
-0.78±0.20(Predicted) | [color ]
Off-White | [InChI]
InChI=1S/C14H10N2O2/c17-13-11-7-4-8-15-12(11)14(18)16(13)9-10-5-2-1-3-6-10/h1-8H,9H2 | [InChIKey]
DWUBVULEMQOCPO-UHFFFAOYSA-N | [SMILES]
C12C(=O)N(CC3=CC=CC=C3)C(=O)C1=CC=CN=2 |
| Hazard Information | Back Directory | [Chemical Properties]
Off-White Solid | [Synthesis]
6-Benzyl-6H-pyrrolo[3,4-B]pyridine-5,7-dione was synthesized using 2,3-pyridinedicarboxylic acid and benzylamine as raw materials by the same method as described previously, and the reaction conditions were adjusted to react at 150 °C for 18-26 hours. After completion of the reaction, the crude product was purified using a 15 cm x 2.5 cm silica gel column with a hexane solution of 60-80% ethyl acetate as eluent. The yield of the purified product was recorded in Table 3. Special note: Saturated NH4Cl solution was used instead of 1 M HCl in the step of washing pyridine derivatives. | [References]
[1] Tetrahedron, 2015, vol. 71, # 48, p. 9101 - 9111
[2] Patent: CN105777750, 2016, A. Location in patent: Paragraph 0024; 0025; 0040
[3] Asian Journal of Chemistry, 2013, vol. 25, # 15, p. 8701 - 8707 |
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