| Identification | Back Directory | [Name]
methyl 8-amino-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylate | [CAS]
248919-96-2 | [Synonyms]
methyl 8-amino-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylate
Imidazo[1,2-a]pyridine-6-carboxylic acid, 8-amino-2,3-dimethyl-, methyl ester | [Molecular Formula]
C11H13N3O2 | [MOL File]
248919-96-2.mol | [Molecular Weight]
219.24 |
| Hazard Information | Back Directory | [Synthesis]
To a suspension of 5,6-diamino-nicotinic acid methyl ester (1 eq., 5.1 g) in cyclohexanone (50 ml) bromobutanone (1.2 equiv., 3.9 ml) was added over 10 min. The mixture was heated to 100° C. (inner temperature) and stirred 2.5 h at this temperature. The mixture was cooled to room temperature and the pale solid methyl 8-amino-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylate was filtered off and was washed with TBME (3×10 ml). Drying under reduced pressure at 45° C. |
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