ChemicalBook--->CAS DataBase List--->2632-65-7

2632-65-7

Request For Quotation
2632-65-7 Structure

2632-65-7 Structure
IdentificationBack Directory
[Name]

4-PYRROLIDIN-1-YLANILINE
[CAS]

2632-65-7
[Synonyms]

AKOS B021942
AKOS BB-8560
TIMTEC-BB SBB009578
ART-CHEM-BB B021942
4-pyrrolidinoaniline
4-PYRROLIDIN-1-YLANILINE
4-(1-PYRROLIDINYL)ANILINE
1-(4-Aminophenyl)pyrrolidine
4-(1-pyrrolidinyl)phenylamine
4-PYRROLIDIN-1-YL-PHENYLAMINE
BenzenaMine,4-(1-pyrrolidinyl)-
[Molecular Formula]

C10H14N2
[MDL Number]

MFCD00156245
[MOL File]

2632-65-7.mol
[Molecular Weight]

162.23
Chemical PropertiesBack Directory
[Melting point ]

51 °C
[Boiling point ]

180-185 °C(Press: 16 Torr)
[density ]

1.109±0.06 g/cm3(Predicted)
[storage temp. ]

under inert gas (nitrogen or Argon) at 2–8 °C
[pka]

7.20±0.40(Predicted)
[Appearance]

Brown to black Solid
Safety DataBack Directory
[Symbol(GHS) ]

Exclamation Mark (GHS07)
GHS07
[Signal word ]

Warning
[Hazard statements ]

H319
[Precautionary statements ]

P305+P351+P338
[HazardClass ]

IRRITANT
[HS Code ]

2933998090
Spectrum DetailBack Directory
[Spectrum Detail]

4-PYRROLIDIN-1-YLANILINE(2632-65-7)1HNMR
Hazard InformationBack Directory
[Synthesis]

1-(4-NITROPHENYL)PYRROLIDINE

10220-22-1

4-PYRROLIDIN-1-YLANILINE

2632-65-7

GENERAL PROCEDURE: The general method for the synthesis of 4-(pyrrolidin-1-yl)aniline from 1-(4-nitrophenyl)pyrrolidine is as follows: 1-(substituted)4-nitrophenyl derivatives IVa, b, e, f (0.01 mol) were dissolved in NH4OH (20 mL, 30%) and an aqueous solution of sodium conidiosulfite (7 g, 0.04 mol) was quickly added (30 mL). The reaction mixture was refluxed for 15 min. After completion of the reaction, the mixture was cooled and the crude product was obtained by filtration. The crude product was washed and crystallized from dichloromethane to give the target compounds Va, b, e, f. Among them, 4-(pyrrolidin-1-yl)aniline Vb was obtained in 80% yield as a yellow oily substance (in agreement with the literature report) [66].

[References]

[1] Bulletin of the Korean Chemical Society, 2015, vol. 36, # 7, p. 1863 - 1873
[2] Bioorganic Chemistry, 2014, vol. 57, p. 65 - 82
[3] Advanced Synthesis and Catalysis, 2018, vol. 360, # 11, p. 2131 - 2137
[4] Patent: US2005/49286, 2005, A1
[5] Justus Liebigs Annalen der Chemie, 1955, vol. 596, p. 1,151
2632-65-7 suppliers list
Company Name: J & K SCIENTIFIC LTD.  
Telephone: 18210857532 18210857532
Website: https://www.jkchemical.com
Company Name: Nanjing Chemlin Chemical Co., Ltd  
Telephone: 025-83697070 13770331960
Website: www.echemlin.cn
Company Name: Chengdu HappySyn Pharmaceutical Technology Co., Ltd.  
Telephone: 85114309 18982182443
Website: www.happysyn.com
Company Name: Chengdu Forest Science and Technology Development Co., Ltd.  
Telephone: 18030648795 18030648795
Website: www.cdforestchem.com
Company Name: Shanghai Xiannuo Biotechnology Co., Ltd.  
Telephone: 021-50718719 13918719472
Website: https://www.chemicalbook.com/ShowSupplierProductsList15633/0_EN.htm
Company Name: Xiamen Dano Pharmaceutical Co., LTD(China)  
Telephone: 0592-6266840 15750707980;
Website: http://www.chemsdano.com
Company Name: Amatek Scientific Co. Ltd.  
Telephone: 0512-56316828 4008675858
Website: http://www.amateksci.com
Company Name: Beijing Wuyunyongchang Science and Technology Co., Ltd.  
Telephone: 15210642910
Website: www.chemicalbook.com/ShowSupplierProductsList16278/0_EN.htm
Company Name: Cool Pharm, Ltd  
Telephone: 021-60455363 18019463053
Website: www.coolpharm.com
Company Name: Nanjing Endesa Bio-tech Co., Ltd.  
Telephone: 025-58862853 18915922038
Website: http://www.endesachem.com
Company Name: Chengdu J&B Technology Co., Ltd.  
Telephone: 028-61186694 15608078506
Website: https://www.chemicalbook.com/ShowSupplierProductsList19082/0_EN.htm
Company Name: Changzhou Hopschain Chemical Co.,Ltd.  
Telephone: 85528066 13775048983
Website: http://www.hopschem.cn
Company Name: Amadis Chemical Company Limited  
Telephone: 571-89925085
Website: http://www.amadischem.com
Company Name: Sichuan BoYou Biotechnology Co., Ltd.  
Telephone: 028-65791793 18140026355
Website: https://www.chemicalbook.com/ShowSupplierProductsList20202/0_EN.htm
Company Name: Jiaxing Deyi Chemical Co., Ltd.  
Telephone: 86-0573-85866609 18367600069
Website: www.chemicalbook.com/supplier/10156672/
Company Name: Wuxi AppTec  
Telephone: 022-59987777 13552403979
Website: www.labnetwork.com
Company Name: Aikon International Limited  
Telephone: 025-58851090 13913916777
Website: www.aikonchem.com
Company Name: Henan Alfachem Co.,Ltd.  
Telephone: 0371-55051623 18137891487
Website: www.chemicalbook.com/supplier/14555231/
Tags:2632-65-7 Related Product Information
1655-55-6