| Identification | Back Directory | [Name]
2-Pyridinecarboximidamide,N-hydroxy-5-methoxy-(9CI) | [CAS]
327056-65-5 | [Synonyms]
N-Hydroxy-5-MethoxypicoliniMidaMide
N-Hydroxy-5-methoxy-2-pyridinecarboximidamide
2-Pyridinecarboximidamide, N-hydroxy-5-methoxy-
2-Pyridinecarboximidamide,N-hydroxy-5-methoxy-(9CI) | [Molecular Formula]
C7H9N3O2 | [MDL Number]
MFCD09910311 | [MOL File]
327056-65-5.mol | [Molecular Weight]
167.17 |
| Chemical Properties | Back Directory | [Boiling point ]
317.5±52.0 °C(Predicted) | [density ]
1.32±0.1 g/cm3(Predicted) | [storage temp. ]
Inert atmosphere,Store in freezer, under -20°C | [pka]
14.21±0.50(Predicted) |
| Hazard Information | Back Directory | [Synthesis]
The general procedure for the synthesis of N-hydroxy-5-methoxy-2-pyridine carboxamides from 5-methoxypicolinonitrile is as follows: using the standard method for the synthesis of kainamidoxime, an ethanol (4 mL) solution of 2-cyano-5-methoxypyridine (270 mg, 2.01 mmol), hydroxylamine hydrochloride (0.457 mL, 5 M, 2.28 mmol), and sodium hydroxide (0.230 mL, 10 N, 2.30 mmol) were mixed and heated to reflux for 24 hours. After standard post-treatment, 79 mg of 5-methoxypyridin-2-ylamidoxime was obtained in 24% yield. | [References]
[1] Patent: US2003/55085, 2003, A1 |
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| Company Name: |
Energy Chemical
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| Tel: |
021-58432009 400-005-6266 |
| Website: |
http://www.energy-chemical.com |
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