| Identification | Back Directory | [Name]
Hydroxyacetic Acid Hydrazide | [CAS]
3530-14-1 | [Synonyms]
Hydroxyacethydrazide
Glicolic Acid Hydrazide
2-hydroxyethanehydrazide
Hydroxyacetic Acid Hydrazide
2-Hydroxy-acetic Acid Hydrazide | [Molecular Formula]
C2H6N2O2 | [MDL Number]
MFCD09840691 | [MOL File]
3530-14-1.mol | [Molecular Weight]
90.08 |
| Chemical Properties | Back Directory | [Appearance]
White Crystalline Solid | [Melting point ]
90-930C | [Boiling point ]
395.0±25.0 °C(Predicted) | [density ]
1.311±0.06 g/cm3(Predicted) | [storage temp. ]
-20°C Freezer, Under Inert Atmosphere | [solubility ]
Acetone, Chloroform, Dichloromethane, Ethyl Acetate, Methanol | [form ]
Solid | [pka]
12.46±0.18(Predicted) | [color ]
White to Off-White | [InChI]
InChI=1S/C2H6N2O2/c3-4-2(6)1-5/h5H,1,3H2,(H,4,6) | [InChIKey]
LIUCWHQVLKSECA-UHFFFAOYSA-N | [SMILES]
C(NN)(=O)CO | [CAS DataBase Reference]
3530-14-1 |
| Hazard Information | Back Directory | [Chemical Properties]
White Crystalline Solid | [Uses]
Hydroxyacetic Acid Hydrazide (cas# 3530-14-1) is a compound useful in organic synthesis. | [Synthesis]
A. Synthesis of 2-hydroxyacetylhydrazine. Ethyl 2-hydroxyacetate (1.00 g, 9.60 mmol), hydrazine (0.324 mg, 10.1 mmol) and ethanol (20 mL) were mixed in a reaction vial, heated to 85 °C and kept for 3 hours. After completion of the reaction, the reaction mixture was concentrated to afford the target compound 2-hydroxyacetylhydrazine (0.702 g, 81% yield). The product was analyzed by mass spectrometry (ESI) and showed m/z 91.1 [M + 1]+. | [References]
[1] Molecules, 2016, vol. 21, # 11,
[2] Patent: WO2008/51493, 2008, A2. Location in patent: Page/Page column 196
[3] Chemical Biology and Drug Design, 2016, vol. 88, # 6, p. 873 - 883
[4] Patent: WO2011/77098, 2011, A1. Location in patent: Page/Page column 150
[5] Combinatorial Chemistry and High Throughput Screening, 2011, vol. 14, # 2, p. 132 - 137 |
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