| Identification | Back Directory | [Name]
2,3-Diaminobenzotrifluoride 97% | [CAS]
360-60-1 | [Synonyms]
3-(trifluoroMethyl)benzene-1
2,3-Diaminobenzotrifluoride97%
2,3-Diaminobenzotrifluoride 97%
3-(Trifluoromethyl)benzene-1,2-diamine
1,2-Benzenediamine, 3-(trifluoromethyl)-
3-(Trifluoromethyl)benzene-1,2-diamine97%
3-(Trifluoromethyl)benzene-1,2-diamine 97%
2,3-Diaminobenzotrifluoride, 3-(Trifluoromethyl)phenylene-1,2-diamine | [Molecular Formula]
C7H7F3N2 | [MDL Number]
MFCD08532495 | [MOL File]
360-60-1.mol | [Molecular Weight]
176.14 |
| Chemical Properties | Back Directory | [Melting point ]
41 °C | [Boiling point ]
125 °C(Press: 14 Torr) | [density ]
1.381±0.06 g/cm3(Predicted) | [storage temp. ]
under inert gas (nitrogen or Argon) at 2–8 °C | [form ]
powder | [pka]
2.94±0.10(Predicted) | [color ]
Yellow |
| Hazard Information | Back Directory | [Synthesis]
Step 4: Synthesis of 3-trifluoromethyl-benzene-1,2-diamine; A suspension of 2-nitro-3-(trifluoromethyl)aniline (0.678 g, 3.2 mmol) formed with 10% palladium/carbon catalyst (0.067 g) in methanol (20 mL) was subjected to a hydrogenation reaction under a hydrogen atmosphere (using a hydrogen balloon) for 2 hours. Upon completion of the reaction, the catalyst was removed by filtration and the solvent was subsequently removed by evaporation under reduced pressure to afford 2,3-diaminobenzotrifluoride as an off-white solid (0.420 g, 73.17% yield). | [References]
[1] Patent: WO2010/115736, 2010, A2. Location in patent: Page/Page column 102
[2] Journal of the Chemical Society, 1952, p. 4078
[3] Patent: US2005/54626, 2005, A1. Location in patent: Page/Page column 46
[4] Patent: US2010/120778, 2010, A1. Location in patent: Page/Page column 21
[5] Journal of Medicinal Chemistry, 2010, vol. 53, # 8, p. 3296 - 3304 |
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J & K SCIENTIFIC LTD.
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Cochemical Ltd.
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Cochemical Ltd.
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029-86115547 17791676824 |
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Cool Pharm, Ltd
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