| Identification | Back Directory | [Name]
ETHYL 3-BROMO-4-HYDROXYBENZOATE | [CAS]
37470-58-9 | [Synonyms]
ETHYL 3-BROMO-4-HYDROXYBENZOATE
3-bromo-4-hydroxyBenzoic acid ethyl ester
Benzoic acid, 3-bromo-4-hydroxy-, ethyl ester | [Molecular Formula]
C9H9BrO3 | [MDL Number]
MFCD06204654 | [MOL File]
37470-58-9.mol | [Molecular Weight]
245.07 |
| Chemical Properties | Back Directory | [Melting point ]
102.2-103.1 °C(Solv: hexane (110-54-3)) | [Boiling point ]
297.9±20.0 °C(Predicted) | [density ]
1.546±0.06 g/cm3(Predicted) | [storage temp. ]
under inert gas (nitrogen or Argon) at 2–8 °C | [pka]
6.82±0.18(Predicted) | [Appearance]
White to off-white Solid |
| Hazard Information | Back Directory | [Synthesis]
Step 2. The compound obtained in step 1 was dissolved in anhydrous ethanol and the reaction mixture was heated to reflux for 1.5 hours. After completion of the reaction, the solvent was removed by rotary evaporator to give ethyl 3-bromo-4-hydroxybenzoate as a white solid (3.24 g, 100% yield). The product was characterized by 1H-NMR (CDCl3): δ 8.17 (s, 1H), 7.95 (d, 1H), 7.68 (d, 1H), 4.29 (q, 2H), 1.32 (t, 3H). | [References]
[1] Patent: WO2007/75896, 2007, A2. Location in patent: Page/Page column 124 |
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