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42172-24-7

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42172-24-7 Structure

42172-24-7 Structure
IdentificationBack Directory
[Name]

Dichloromethanesulfenyl chloride
[CAS]

42172-24-7
[MOL File]

42172-24-7.mol
Chemical PropertiesBack Directory
[Boiling point ]

30 °C(Press: 10 Torr)
[density ]

1.6143 g/cm3(Temp: 34 °C)
Questions And Answer(Q&A)Back Directory
[Preparation]

To an ice-cooled dry flask containing 25.0 gm (0.18 mole) of s-trithiane is slowly added dry chlorine gas. As soon as the solid liquefies, the temperature is raised to 10-20°C, and approximately a total of 57.0 gm (0.80 mole) of chlorine gas is absorbed. The product is distilled under reduced pressure to afford 9.9-12.9 gm (46-60%), b.p. 30°C (10 mm Hg).
Preparation of Dichloromethanesulfenyl Chloride
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