| Identification | Back Directory | [Name]
2,6-Dimethyl-4-bromobenzaldehyde | [CAS]
5769-33-5 | [Synonyms]
2,6-Dimethyl-4-bromobenzaldehyde
4-Bromo-2,6-dimethylbenzaldehyde
Benzaldehyde, 4-bromo-2,6-dimethyl-
tert-butyl 3-allyl-3-hydroxyazetidine-102-carboxylate | [Molecular Formula]
C9H9BrO | [MDL Number]
MFCD11227151 | [MOL File]
5769-33-5.mol | [Molecular Weight]
213.07 |
| Chemical Properties | Back Directory | [Boiling point ]
137-139 °C(Press: 12 Torr) | [density ]
1.422±0.06 g/cm3(Predicted) | [storage temp. ]
under inert gas (nitrogen or Argon) at 2-8°C | [Appearance]
Off-white to light brown Solid |
| Hazard Information | Back Directory | [Synthesis]
1. 5-bromo-2-iodo-1,3-xylene is dissolved in anhydrous N,N-dimethylformamide under nitrogen protection.
2. a palladium catalyst and an appropriate amount of base are added, and the reaction is heated to 80-100°C for 12-24 hours.
3. After completion of the reaction, cool to room temperature, dilute with water and extract with an organic solvent.
4. The organic layers were combined, dried with anhydrous sodium sulfate, filtered and concentrated.
5. Purify the crude product by column chromatography to obtain 4-bromo-2,6-dimethylbenzaldehyde. | [References]
[1] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2016, vol. 55B, # 7, p. 854 - 881 |
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