ChemicalBook--->CAS DataBase List--->630384-36-0

630384-36-0

630384-36-0 Structure

630384-36-0 Structure
IdentificationBack Directory
[Name]

Cyclopropanecarboxylic acid, 1-(4-iodophenyl)-, methyl ester
[CAS]

630384-36-0
[Synonyms]

Methyl 1-(4-iodophenyl)cyclopropanecarboxylate
METHYL 1-(4-IODOPHENYL)CYCLOPROPANE-1-CARBOXYLATE
1-(4-iodophenyl)cyclopropanecarboxylic acid methyl ester
Cyclopropanecarboxylic acid, 1-(4-iodophenyl)-, methyl ester
CYCLOPROPANECARBOXYLIC ACID, 1-(4-IODOPHENYL)-, MEHTYL ESTER
[Molecular Formula]

C11H11IO2
[MDL Number]

MFCD15523646
[MOL File]

630384-36-0.mol
[Molecular Weight]

302.11
Chemical PropertiesBack Directory
[storage temp. ]

2-8°C(protect from light)
Hazard InformationBack Directory
[Synthesis]

Methanol

67-56-1

1-(4-iodophenyl)cyclopropane-1-carboxylic acid

124276-89-7

Cyclopropanecarboxylic acid, 1-(4-iodophenyl)-, methyl ester

630384-36-0

Chlorotrimethylsilane (0.33 g, 3 mmol) was slowly added dropwise to a solution of 1-(4-iodophenyl)cyclopropanecarboxylic acid (0.86 g, 3 mmol) in methanol (15 mL) at 0 °C. After the dropwise addition, the reaction mixture was stirred at room temperature overnight. After completion of the reaction, the solvent was removed by vacuum evaporation to afford methyl 1-(4-iodophenyl)cyclopropanecarboxylate (0.9 g, 100% yield).

[References]

[1] Patent: WO2013/25733, 2013, A1. Location in patent: Paragraph 0609
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