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696-01-5

696-01-5 Structure

696-01-5 Structure
IdentificationBack Directory
[Name]

2-Fluoro-p-Xylene
[CAS]

696-01-5
[Synonyms]

1,4-Dimethyl-2-fluorobenzene
[Molecular Formula]

C8H9F
[MDL Number]

MFCD03412243
[MOL File]

696-01-5.mol
[Molecular Weight]

124.16
Chemical PropertiesBack Directory
[Melting point ]

-6℃
[Boiling point ]

144.7℃
[density ]

0.983
[Fp ]

30.9℃
[storage temp. ]

Sealed in dry,Room Temperature
[solubility ]

Acetonitrile (Slightly), Chloroform (Slightly)
[form ]

liquid
[color ]

Pale yellow
Safety DataBack Directory
[Symbol(GHS) ]

Flame (GHS02)Exclamation Mark (GHS07)
GHS02,GHS07
[Signal word ]

Warning
[Hazard statements ]

H226-H315-H319-H335
[Precautionary statements ]

P210-P261-P280
[HS Code ]

2903998090
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Calcium chloride-->Fluoroboric acid-->2,5-Dimethylaniline-->Sodium nitrite-->2,5-Dimethylnitrobenzene
[Preparation Products]

Benzene, 1-(fluoromethyl)-4-methyl--->3-Fluoro-4-methylbenzoic acid-->2-Chloro-1,4-dimethylbenzene-->p-Fluorotoluene-->P-XYLENE-->2,5-Dimethylphenol
Hazard InformationBack Directory
[Chemical Properties]

liquid. Boiling point 137-138℃.
[Uses]

2-Fluoro-p-Xylene can be used to prepare phase transfer catalyst 2-fluoro-4-methylbenzyltrimethylammonium bromide.
[Synthesis]

2-Fluoro-p-Xylene was prepared by Schiemann reaction of 2,5-dimethylaniline.
[References]

[1] Patent: US6179970, 2001, B2
[2] European Journal of Medicinal Chemistry, 2004, vol. 39, # 7, p. 573 - 578
[3] Journal of the American Chemical Society, 1950, vol. 72, p. 4809
[4] Journal of the Chemical Society, Chemical Communications, 1978, p. 992 - 993
[5] Journal of Organic Chemistry, 1967, vol. 32, p. 134 - 136
Spectrum DetailBack Directory
[Spectrum Detail]

2-Fluoro-p-Xylene(696-01-5)1HNMR
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