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73500-82-0

73500-82-0 Structure

73500-82-0 Structure
IdentificationBack Directory
[Name]

CARBAZOLE-N-CARBONYL CHLORIDE
[CAS]

73500-82-0
[Synonyms]

9-(CHLOROFORMYL)CARBAZOLE
N-(CHLOROCARBONYL)CARBAZOLE
9-(Chlorocarbonyl)carbazole
9-(Chloroformyl)-9H-carbazole
CARBAZOLE-N-CARBONYL CHLORIDE
CARBAZOLE-9-CARBONYL CHLORIDE
9H-Carbazole-9-carbonyl chloride
Carbazole-9-carbonyl Chloride >
9H-Carbazole-9-carboxylic acid chloride
CARBAZOLE-9-CARBONYL CHLORIDE, FOR FLUOR ESCENCE
CARBAZOLE-N-CARBONYL CHLORIDE ISO 9001:2015 REACH
[Molecular Formula]

C13H8ClNO
[MDL Number]

MFCD00059689
[MOL File]

73500-82-0.mol
[Molecular Weight]

229.66
Chemical PropertiesBack Directory
[Melting point ]

100-104 °C
[Boiling point ]

407.5±28.0 °C(Predicted)
[density ]

1.32±0.1 g/cm3(Predicted)
[storage temp. ]

2-8°C
[form ]

powder to crystal
[color ]

White to Almost white
[CAS DataBase Reference]

73500-82-0
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

36/38
[Safety Statements ]

26-36
[WGK Germany ]

3
[F ]

10-21
[HS Code ]

2928.00.5000
Hazard InformationBack Directory
[Purification Methods]

Recrystallise the acid chloride from *C6H6. If it is not very pure (presence of OH or NH bands in the IR), dissolve it in pyridine, shake it with phosgene in toluene, evaporate and recrystallise the residue. Carry out this experiment in a good fume cupboard as COCl2 is very TOXIC, and store the product in the dark. It is moisture sensitive. The amide has m 246.5-247o, and the dimethylaminoethylamide hydrochloride has m 197-198o. [Weston et al. J Am Chem Soc 75 4006 1953, Beilstein 20 III/IV 3841.]
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