| Identification | Back Directory | [Name]
4,4'-oxybisbutan-2-ol | [CAS]
821-33-0 | [Synonyms]
Diskin
Boutybil
Dis-Cinil
Dyskinebyl
Diskinebyl
Colenormol
Einecs 212-475-3
5-Oxa-2,8-nonandiol
4,4'-oxydi-2-butanol
4,4'-oxybisbutan-2-ol
4,4'-Oxybis(2-butanol)
2-Butanol, 4,4'-oxybis-
3,3-Dihydroxydibutyl ether
Dibutyl 3,3''-dihydroxy ether
4-(3-hydroxybutoxy)butan-2-ol
Dihydroxydibutylether (DHDB-N)
1,1'-Dimethyl-3,3'-oxydipropanol | [EINECS(EC#)]
212-475-3 | [Molecular Formula]
C8H18O3 | [MDL Number]
MFCD19301161 | [MOL File]
821-33-0.mol | [Molecular Weight]
162.23 |
| Hazard Information | Back Directory | [Originator]
Dyskineacutebyl,Saunier | [Definition]
ChEBI: Oxydibutanol is a secondary alcohol. | [Manufacturing Process]
To a solution of 3 mols butylmagnesiumbromide in ether was added dropwise an one mol of β-cyanoethyloxide. The mixture was refluxed for 1 hour. Then after cooling to the mixture was added hydrochloric acid. An organic layer was dried under sodium sulfate and evaporated. An oil layer was distilled in vacuum. The oxo-3-butane oxide has a boiling point 123-125°C at 15 mm.
A mixture of 100 g of oxo-3-butane oxide, 500 ml ethanol and 15 g Nickel Reney was loaded in autoclave and heated at 45-50°C. In autoclave was introduced a hydrogene. After cooling the mixture was filtered and ethanol was distilled off. 1,1'-Dimethyl-3,3'-oxydipropanol was distilled at 160161°C/18 mm.
| [Therapeutic Function]
Choleretic, Spasmolytic |
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