| Identification | Back Directory | [Name]
3- BROMO-2-METHYL- BENZALDEHYDE | [CAS]
83647-40-9 | [Synonyms]
3-broMo-2-tolualdehyde
3-Bromo-2-methylbenzaldehyde97%
Benzaldehyde, 3-bromo-2-methyl-
3- BROMO-2-METHYL- BENZALDEHYDE
3-Bromo-2-methylbenzaldehyde 97%
3-Bromo-o-tolualdehyde, 2-Bromo-6-formyltoluene
3- BROMO-2-METHYL- BENZALDEHYDE ISO 9001：2015 REACH | [EINECS(EC#)]
200-258-5 | [Molecular Formula]
C8H7BrO | [MDL Number]
MFCD11847533 | [MOL File]
83647-40-9.mol | [Molecular Weight]
199.045 |
| Chemical Properties | Back Directory | [Boiling point ]
255.3±20.0 °C(Predicted) | [density ]
1.490±0.06 g/cm3(Predicted) | [storage temp. ]
Inert atmosphere,2-8°C | [form ]
fused solid | [color ]
Clear, orange/amber liquid |
| Hazard Information | Back Directory | [Synthesis]
(3-Bromo-2-methylphenyl)methanol (24 g, 119 mmol) was dissolved in dichloromethane (240 mL) and manganese (IV) oxide (103 g, 1.2 mol). After stirring overnight, TLC showed no starting material. The reaction mixture was evaporated with silica gel and loaded on a small silica gel column. After evaporation, the product was eluted with hexane:ethyl acetate (10:1) to give pure aldehyde 3-bromo-2-methylbenzaldehyde (18.6 g).
| [References]
[1] Patent: US2010/160303, 2010, A1. Location in patent: Page/Page column 36
[2] Journal of the American Chemical Society,
[3] Journal of the American Chemical Society, 2009, vol. 131, p. 1410 - 1412
[4] Journal of the American Chemical Society, 2010, vol. 132, # 1, p. 371 - 383
[5] Patent: WO2010/143733, 2010, A1. Location in patent: Page/Page column 347-348 |
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| Company Name: |
Energy Chemical
|
| Telephone: |
400-0056266 |
| Website: |
www.energy-chemical.com |
| Company Name: |
Struchem Co., Ltd.
|
| Telephone: |
0512-63009836 18994340901 |
| Website: |
http://www.beidapharma.com |
|