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87950-39-8

87950-39-8 Structure

87950-39-8 Structure
IdentificationBack Directory
[Name]

4-(3,4-DIACETOXYBENZAL)-2-METHYL-5-OXAZOLONE
[CAS]

87950-39-8
[Synonyms]

4-(3,4-DIACETOXYBENZAL)-2-METHYL-5-OXAZOLONE
4-[[3,4-Bis(acetyloxy)phenyl]Methylene]-2-Methyl-5(4H)-oxazolone
[Molecular Formula]

C15H13NO6
[MOL File]

87950-39-8.mol
[Molecular Weight]

303.267
Questions And AnswerBack Directory
[Synthesis]

In a 500mL three-necked flask, 55.2g of 3,4-dihydroxybenzaldehyde, 56.7g of acetaminophen, 42.6g of anhydrous sodium acetate, and 204.2g of freshly distilled acetic anhydride were added. The mixture was stirred at 80℃ for 5 hours. After cooling to room temperature, 150mL of ice water was added to the reaction solution, and the mixture was stirred until a homogeneous emulsion was formed. Upon cooling, a large amount of yellow crystals precipitated. The crystals were filtered, washed, and dried to obtain 98.0g of yellow crystals (mp 161.0℃~161.4℃), with a yield of 80.9%.

Synthesis of 87950-39-8

Chemical PropertiesBack Directory
[Appearance]

Yellow Solid
[Boiling point ]

448.3±55.0 °C(Predicted)
[density ]

1.31±0.1 g/cm3(Predicted)
[solubility ]

Dichloromethane, Ethyl Acetate
[form ]

Solid
[pka]

0.62±0.20(Predicted)
[color ]

Yellow
[CAS DataBase Reference]

87950-39-8
Hazard InformationBack Directory
[Chemical Properties]

Yellow Solid
[Uses]

4-(3,4-Diacetoxybenzal)-2-methyl-5-oxazolone (cas# 87950-39-8) is a compound useful in organic synthesis.
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