| Identification | Back Directory | [Name]
6-BROMO-4-METHYLQUINOLIN-2(1H)-ONE | [CAS]
89446-19-5 | [Synonyms]
6-Bromo-4-methyl-2-quinolinol
6-BROMO-4-METHYLQUINOLIN-2(1H)-ONE
6-Bromo-4-methyl-2(1H)-quinolinone
2(1H)-Quinolinone, 6-bromo-4-methyl-
6-broMo-4-Methyl-1,2-dihydroquinolin-2-one
6-bromo-4-methyl-2(1H)-quinolinone(SALTDATA: FREE) | [Molecular Formula]
C10H8BrNO | [MDL Number]
MFCD11053820 | [MOL File]
89446-19-5.mol | [Molecular Weight]
238.08 |
| Chemical Properties | Back Directory | [Melting point ]
290-292 °C | [Boiling point ]
392.6±42.0 °C(Predicted) | [density ]
1.523±0.06 g/cm3(Predicted) | [storage temp. ]
Sealed in dry,Room Temperature | [pka]
10.79±0.70(Predicted) | [Appearance]
White to light brown Solid |
| Hazard Information | Back Directory | [Synthesis]
(b) N-(4-bromophenyl)-3-oxobutanamide (0.73 g, 2.85 mmol) was dissolved in concentrated hydrochloric acid. The reaction was heated to 120 °C in an oil bath and sodium sulfate (7 mL) was added and kept at this temperature for 1 hour. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently poured into a beaker containing ice. The precipitate precipitated was collected by filtration to afford 6-bromo-4-methyl-2(1H)-quinolinone as a tan solid (0.4 g, 60% yield). | [References]
[1] Patent: WO2010/132615, 2010, A1. Location in patent: Page/Page column 138
[2] Synthesis, 2011, # 6, p. 934 - 942
[3] Patent: US2005/234101, 2005, A1. Location in patent: Page/Page column 14
[4] Patent: WO2005/103002, 2005, A2. Location in patent: Page/Page column 44
[5] Patent: US2005/267115, 2005, A1. Location in patent: Page/Page column 21 |
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| Company Name: |
Energy Chemical
|
| Tel: |
021-021-58432009 400-005-6266 |
| Website: |
http://www.energy-chemical.com |
| Company Name: |
NovoChemy Ltd.
|
| Tel: |
021-31261262/ 49 (0)17662837245 |
| Website: |
www.novochemy.com |
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