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97611-55-7

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97611-55-7 Structure

97611-55-7 Structure
IdentificationBack Directory
[Name]

2-ACETOXY-N-(DIPHENYLMETHYLENE)GLYCINE ETHYL ESTER
[CAS]

97611-55-7
[Synonyms]

Ethyl N-(Diphenylmethylene)-2-acetoxyglycinate
ethyl 2-acetoxy-2-diphenylmethyleneaminoacetate
2-ACETOXY-N-(DIPHENYLMETHYLENE)GLYCINE ETHYL ESTER
Acetic acid, 2-(acetyloxy)-2-[(diphenylmethylene)amino]-, ethyl ester
[Molecular Formula]

C19H19NO4
[MOL File]

97611-55-7.mol
[Molecular Weight]

325.36
Chemical PropertiesBack Directory
[Boiling point ]

421.0±45.0 °C(Predicted)
[density ]

1.11±0.1 g/cm3(Predicted)
[pka]

0.60±0.50(Predicted)
Hazard InformationBack Directory
[Preparation]

2-Acetoxy-n-(diphenylmethylene)glycine ethyl ester is prepares by bromination of ethyl N-(diphenylmethylene)glycinate in the presence of  acetate (NBS, NaOAc, DMF).1 The crude product can be purified by recrystalization. (Et2O/hexane)
[storage]

Although stable at room temperature, the compound is normally  stored under argon in the freezer. The hydrolysis product, benzophenone, can be detected either by TLC  (EtOAc/hexane) or by NMR.
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