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ChemicalBook >> CAS DataBase List >>6-Bromo-3-hydroxypicolinicacid

6-Bromo-3-hydroxypicolinicacid

6-Bromo-3-hydroxypicolinicacid Structure
6-Bromo-3-hydroxypicolinicacid structure
CAS No.
321596-58-1
Chemical Name:
6-Bromo-3-hydroxypicolinicacid
Synonyms
6-Bromo-3-hydroxypicolinicacid;6-BroMo-3-hydroxypyridine-2-carboxylic acid;2-Pyridinecarboxylic acid, 6-bromo-3-hydroxy-
CBNumber:
CB22499101
Molecular Formula:
C6H4BrNO3
Molecular Weight:
218
MDL Number:
MFCD18072573
MOL File:
321596-58-1.mol
Last updated:2025-07-24 18:13:47
Product description Number Pack Size Price
6-Bromo-3-hydroxypicolinicAcid B993745 100mg $200
6-Bromo-3-hydroxypicolinicAcid B993745 50mg $130
6-Bromo-3-hydroxypicolinic acid 95+% 076584 1g $329
6-Bromo-3-hydroxypicolinic acid 95+% 076584 500mg $214
6-Bromo-3-hydroxypicolinicacid W5403 250mg $398.8
Request For Quotation

6-Bromo-3-hydroxypicolinicacid Properties

Boiling point 485.7±45.0 °C(Predicted)
Density 1.985±0.06 g/cm3(Predicted)
storage temp. under inert gas (nitrogen or Argon) at 2-8°C
pka 2.32±0.25(Predicted)
Appearance Off-white to light yellow Solid

6-Bromo-3-hydroxypicolinicacid price More Price(17)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TRC B993745 6-Bromo-3-hydroxypicolinicAcid 321596-58-1 100mg $200 2021-12-16 Buy
TRC B993745 6-Bromo-3-hydroxypicolinicAcid 321596-58-1 50mg $130 2021-12-16 Buy
Matrix Scientific 076584 6-Bromo-3-hydroxypicolinic acid 95+% 321596-58-1 1g $329 2021-12-16 Buy
Matrix Scientific 076584 6-Bromo-3-hydroxypicolinic acid 95+% 321596-58-1 500mg $214 2021-12-16 Buy
AK Scientific W5403 6-Bromo-3-hydroxypicolinicacid 321596-58-1 250mg $398.8 2021-12-16 Buy
Product number Packaging Price Buy
B993745 100mg $200 Buy
B993745 50mg $130 Buy
076584 1g $329 Buy
076584 500mg $214 Buy
W5403 250mg $398.8 Buy

6-Bromo-3-hydroxypicolinicacid Chemical Properties,Uses,Production

Synthesis

3-Hydroxypicolinic acid

874-24-8

6-Bromo-3-hydroxypicolinicacid

321596-58-1

General procedure for the synthesis of 6-bromo-3-hydroxypyridine-2-carboxylic acid from 3-hydroxy-2-pyridinecarboxylic acid: to a stirred suspension of 3-hydroxypyridine-2-carboxylic acid (2.00 g, 0.0144 mol) in DMF (30 mL) was slowly added a solution of N-bromosuccinimide (2.56 g, 0.0144 mol) in DMF (30 mL). After 1 h of reaction, water (50 mL) and 1 M NaOH aqueous solution (25 mL) were added, followed by extraction of the reaction mixture with chloroform (3 x 150 mL). The organic layers were combined and concentrated under reduced pressure and the resulting residue was purified by preparative HPLC (System D). The final product 6-bromo-3-hydroxypyridine-2-carboxylic acid was obtained as 366 mg in 12% yield. The product was assayed by analytical HPLC and the purity was 100% in both cases (System A and B); LRESIMS (ESI+) m/z = 218/220 (M + H)+.

References

[1] Patent: WO2009/150144, 2009, A1. Location in patent: Page/Page column 63

6-Bromo-3-hydroxypicolinicacid Preparation Products And Raw materials

Raw materials

3-Hydroxypicolinic acid N,N-Dimethylformamide Water N-Bromosuccinimide Sodium hydroxide

Preparation Products

6-Bromo-3-hydroxypicolinicacid Suppliers

Global( 29)Suppliers
Supplier Tel Email Country ProdList Advantage
Alchem Pharmtech,Inc. 		8485655694 sales@alchempharmtech.com United States 63687 58
Suzhou ARTK Medchem Co., Ltd. 		+86-512-68323658 +86-18168183658 sales1@artkmedchem.com China 39002 58
Cochemical Co. Ltd. 		+86-029-86115547 +86-17791676824 sales@cochemical.com China 3952 58
Amadis Chemical Company Limited 		571-89925085 sales@amadischem.com China 131957 58
Chiba Pharmaceutical Science and technology Co, Ltd. 0531-81313138 13066006660 chibapharm@foxmail.com China 3966 55
Shanghai Topbiochem Technology Co., Ltd +86-21-60341587 sales@topbiochem.com China 6175 58
Shanghai Witofly Chemical Co.,Ltd sales@witofly.com China 2864 52
Cochemical Ltd. 029-86115547 17791676824 sales@cochemical.com China 3014 58
Shanghai Anmike Chemical Co. Ltd. 微信 17321281695 18019252918 sale@amkchem.com China 9991 55
Nanijing m&m biotechnology Co. ,Ltd. 025-87782433 18021532344 1345332203@qq.com China 4158 58
Supplier Advantage
Alchem Pharmtech,Inc. 		58
Suzhou ARTK Medchem Co., Ltd. 		58
Cochemical Co. Ltd. 		58
Amadis Chemical Company Limited 		58
Chiba Pharmaceutical Science and technology Co, Ltd. 55
Shanghai Topbiochem Technology Co., Ltd 58
Shanghai Witofly Chemical Co.,Ltd 52
Cochemical Ltd. 58
Shanghai Anmike Chemical Co. Ltd. 55
Nanijing m&m biotechnology Co. ,Ltd. 58

6-Bromo-3-hydroxypicolinicacid Spectrum

6-Bromo-3-hydroxypicolinicacid(321596-58-1)1HNMR

321596-58-1(6-Bromo-3-hydroxypicolinicacid)Related Search:

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6-Bromo-3-hydroxypicolinicacid 6-BroMo-3-hydroxypyridine-2-carboxylic acid 2-Pyridinecarboxylic acid, 6-bromo-3-hydroxy- 321596-58-1