(10-Phenyl-9-anthracenyl)boronic acid pinacol ester
- CAS No.
- 460347-59-5
- Chemical Name:
- (10-Phenyl-9-anthracenyl)boronic acid pinacol ester
- Synonyms
- 10-Phenylanthracene-9-boronic Acid Pinacol Ester;(10-Phenyl-9-anthracenyl)boronic acid pinacol ester;9-Phenyl-10-anthracen(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl);9-Phenyl-10-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)anthracene;4,4,5,5-Tetramethyl-2-(10-phenyl-9-anthracenyl)-1,3,2-dioxaborolane;4,4,5,5-Tetramethyl-2-(10-Phenylanthracen-9-Yl)-1,3,2-Dioxaborolane;4,4,5,5-tetramethyl-2-(9-phenylanthracen-10-yl)-1,3,2-dioxaborolane;9-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-10-phenylanthracene;1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-(10-phenyl-9-anthracenyl)-
- CBNumber:
- CB52462210
- Molecular Formula:
- C26H25BO2
- Molecular Weight:
- 380.29
- MDL Number:
- MFCD13194955
- MOL File:
- 460347-59-5.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS07 |
---|---|
Signal word | Warning |
Hazard statements | H302-H315-H319-H335 |
Precautionary statements | P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 |
HS Code | 2931.90.6000 |
(10-Phenyl-9-anthracenyl)boronic acid pinacol ester price More Price(11)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
TCI Chemical | T3665 | 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane >98.0%(GC) | 460347-59-5 | 1g | $43 | 2024-03-01 | Buy |
TCI Chemical | T3665 | 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane >98.0%(GC) | 460347-59-5 | 5g | $173 | 2024-03-01 | Buy |
TRC | T889730 | 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane | 460347-59-5 | 100mg | $75 | 2021-12-16 | Buy |
Chem-Impex | 40044 | 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane,98%(GC) 98%(GC) | 460347-59-5 | 1G | $236.32 | 2021-12-16 | Buy |
Chem-Impex | 40044 | 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane,≥98%(GC) ≥98%(GC) | 460347-59-5 | 5G | $830.5 | 2021-12-16 | Buy |
(10-Phenyl-9-anthracenyl)boronic acid pinacol ester Chemical Properties,Uses,Production
Preparation
9-Bromo-10-phenylanthracene (5.8g, 17.4mmol), bis(pinacolato)diboron(6.63 g, 26.1 mmol), Pd(dppf)Cl2 (710 mg, 0.87 mmol), and KOAc (10.23 g, 104.4 mmol) were mixed in a 250mL flask containing 1,4-dioxane (60 mL). The reaction mixture was refluxed for 24h under nitrogen. After it was cooled to room temperature, a dilute hydrochloric acid solution quenched. The mixture was extracted with CH2Cl2 and dried over anhydrous MgSO4. The crude product was concentrated by rotary evaporation and further purified by silica gel column chromatography (CH2Cl2 / petroleum ether (1:1,v/v)) to afford a light yellow powder (4.0 g, 60.4 %). 1H NMR (500 MHz, CDCl3) δ 8.46 (d, J = 8.7 Hz, 2H), 7.65 (d, J = 8.8 Hz, 2H), 7.57 (dq, J = 14.2, 7.0 Hz, 3H), 7.51 – 7.46 (m, 2H), 7.41 (d, J = 7.0 Hz, 2H), 7.34 (dd, J = 8.1, 7.1 Hz, 2H), 1.63 (s, 12H). EI-MS (m/z): Calculated for C26H25BO2: 380.29. Found [M+]: 379.92.
Synthesis of 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane
(10-Phenyl-9-anthracenyl)boronic acid pinacol ester Preparation Products And Raw materials
Raw materials
Preparation Products
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 | info@dakenam.com | China | 18628 | 58 |
ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32836 | 60 |
SHAANXI WEISHINUO THE NEW MATERIALCO,.LTD | 18792503214 | Beryl@weishino.com | CHINA | 256 | 58 |
BAYNOE CHEM CO.,LTD | +86-21-34783353 +8615000719740 | baynoe@baynoe.com | CHINA | 934 | 58 |
career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29823 | 58 |
Richest Group Ltd | 18017061086 | oled@richest-group.com | CHINA | 5601 | 58 |
CD Chemical Group Limited | +8615986615575 | info@codchem.com | China | 20356 | 58 |
Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418684 +8618949823763 | sales@tnjchem.com | China | 25363 | 58 |
Hangzhou MolCore BioPharmatech Co.,Ltd. | +86-057181025280; +8617767106207 | sales@molcore.com | China | 49739 | 58 |
Shaoxin Catsyn Co., Ltd. | +undefined-0575-82040869 +86-0575-82040869; | sales@catsyn.com | China | 6116 | 58 |
View Lastest Price from (10-Phenyl-9-anthracenyl)boronic acid pinacol ester manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
---|---|---|---|---|---|---|---|---|
2024-09-09 | 4,4,5,5-tetramethyl-2-(9-phenylanthracen-10-yl)-1,3,2-dioxaborolane
460347-59-5
|
US $0.00 / KG | 1KG | 98.00% | 150KG /month | Shanghai Daken Advanced Materials Co.,Ltd | ||
2020-01-10 | (10-Phenyl-9-anthracenyl)boronic acid pinacol ester
460347-59-5
|
US $1.00 / KG | 1KG | 98% HPLC | 10 tons/month | Career Henan Chemical Co |
- 4,4,5,5-tetramethyl-2-(9-phenylanthracen-10-yl)-1,3,2-dioxaborolane
460347-59-5
- US $0.00 / KG
- 98.00%
- Shanghai Daken Advanced Materials Co.,Ltd
- (10-Phenyl-9-anthracenyl)boronic acid pinacol ester
460347-59-5
- US $1.00 / KG
- 98% HPLC
- Career Henan Chemical Co