3-(3-(Trifluoromethyl)phenyl)propanal
3-(3-(Trifluoromethyl)phenyl)propanal 物理性質
- 沸点 :
- 207.4±35.0 °C(Predicted)
- 比重(密度) :
- 1.192±0.06 g/cm3(Predicted)
- 貯蔵温度 :
- Inert atmosphere,Store in freezer, under -20°C
- 溶解性:
- クロロホルム、ジクロロメタン、酢酸エチルに可溶
- 外見 :
- 油
- 色:
- 無色透明~淡黄色の油状液体
- 安定性::
- 安定性が低く、室温を維持した場合の TLC の新しいスポット。
- InChI:
- InChI=1S/C10H9F3O/c11-10(12,13)9-5-1-3-8(7-9)4-2-6-14/h1,3,5-7H,2,4H2
- InChIKey:
- APCCHYPQHODSBD-UHFFFAOYSA-N
- SMILES:
- C1(CCC=O)=CC=CC(C(F)(F)F)=C1
3-(3-(Trifluoromethyl)phenyl)propanal 価格
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3-(3-(Trifluoromethyl)phenyl)propanal 化学特性,用途語,生産方法
化学的特性
Colourless Oil
使用
3-(Trifluoromethyl)benzenepropanal (cas# 21172-41-8) is a compound useful in organic synthesis.
合成
A solution of 3-(Trifluoromethyl) benzene propanol (1.0 g, 4.90 mmol) in dichloromethane (20 ml) is cooled in a water/ice bath, treated in succession with DMSO (770 mg, 9.80 mmol) and P2O5 (1.39 g, 9.80 mmol) and left under stirring for 30 minutes, while temperature raises to 20°C. The reaction mixture is then cooled in water/ice bath and triethylamine (2.4 ml, 17.15 mmol). The resulting solution is kept under stirring while the temperature raises to 20°C. After one hour, the mixture is treated with 5 per cent HCl, the phases are separated, and the organic one is further washed with 5 per cent HCl. The organic phase is then washed with brine, dried over Na2SO4, filtered and concentrated under reduced pressure to afford 0.99 g of the aldehyde of 3-(3-(Trifluoromethyl)phenyl)propanal in quantitative yield.
3-(3-(Trifluoromethyl)phenyl)propanal 上流と下流の製品情報
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準備製品
3-(3-(Trifluoromethyl)phenyl)propanal 生産企業
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21172-41-8()キーワード:
- 21172-41-8
- 3-(3-TRIFLUOROMETHYL-PHENYL)-PROPIONALDEHYDE
- 3-(Trifluoromethyl)benzenepropanal
- m-(Trifluoromethyl)hydrocinnamaldehyde
- 4-[3-(trifluoroMethyl)phenyl]butanal
- Benzenepropanal, 3-(trifluoroMethyl)-
- 3-(trifluoroMethylphenyl)propionaldehyde
- 3-(3-TRIFLUOROMETHYL-PHENYL)-PROPIOLDEHYDE
- Cinacalcet Impurity 54
- 3-(3-(trifluoroMethyl)phenyl)propanal