Trihexylboron

Trihexylboron C화학적 특성, 용도, 생산

Purification Methods

Treat the borane with hex-1-ene and 10% anhydrous Et2O for 6hours at gentle reflux under N2, then distil it in a vacuum through an 18inch glass helices-packed column under N2 taking the fraction b 130o/2.1mm to 137o/1.5mm. The distillate may still contain some di-n-hexylborane [Brown & Subba Rao J Am Chem Soc 81 6423 1959, Mirviss J Am Chem Soc 83 3051 1961]. [Beilstein 4 IV 4362.]

Trihexylboron 준비 용품 및 원자재

원자재

준비 용품

Trihexylboron 공급 업체

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