2,3,6,7,14,15-Hexabromo-9,10-dihydro-9,10-[1,2]benzenoanthracene
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2,3,6,7,14,15-Hexabromo-9,10-dihydro-9,10-[1,2]benzenoanthracene 속성
- 녹는점
- >350 °C(Solv: acetone (67-64-1))
- 끓는 점
- 552.6±50.0 °C(Predicted)
- 밀도
- 2.351±0.06 g/cm3(Predicted)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
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유해·위험 문구: |
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예방조치문구: |
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2,3,6,7,14,15-Hexabromo-9,10-dihydro-9,10-[1,2]benzenoanthracene C화학적 특성, 용도, 생산
용도
2,3,6,7,14,15-Hexabromo-9,10-dihydro-9,10-[1,2]benzenoanthracene can be used as impurity standard and reference substance, mainly used in laboratory research and development process and chemical production process middle.Synthesis
Triptycene (1.06 g, 4.18 mmol) was dissolved in chloroform (80 mL) in a round-bottom flask. Iron filings (30 mg) were added, and the solution was stirred at 25 ??C. Bromine (1.35 mL, 26.3 mmol) was added, and the solution was refluxed for 1 h, during which time the initially reddish-brown solution turned reddish-orange. The flask was removed from heat, and chloroform and excess bromine were removed under vacuum. The resulting brown powder was dissolved in chloroform (100 mL) and flushed through a pad of silica using additional chloroform as eluent (100 mL). The filtrate was evaporated to dryness. The crude white powder (2.83 g, 98%) was crystallized from acetone yielding C20H8Br6 ?¤ (acetone)2 (0.88 g, 29%), mp >350 ??C. The mother liquor was evaporated and the residue was crystallized from acetone to afford a second crop of crystals (0.97 g, C20H8Br6 ?¤ (acetone)2, 32%). The combined yield was 1.85 g, 61%: 2-H yield 2.83 g, 98%
2,3,6,7,14,15-Hexabromo-9,10-dihydro-9,10-[1,2]benzenoanthracene 준비 용품 및 원자재
원자재
준비 용품
2,3,6,7,14,15-Hexabromo-9,10-dihydro-9,10-[1,2]benzenoanthracene 공급 업체
글로벌( 42)공급 업체
공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
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Jilin Chinese Academy of Sciences - Yanshen Technology Co., Ltd. | 0431-80514535 13634302652 |
Extension@chemextension.com | CHINA | 967 | 58 |
CHEMSOON CO.,LTD. | +8613761723174 |
sales01@chemsoon.com | China | 1211 | 58 |
Zhengzhou Alfa Chemical Co.,Ltd | +8618530059196 |
sale04@alfachem.cn | China | 12550 | 58 |
Shanghai Daeyeon Chemicals Co., Ltd | 021-64478606 +8615900664856 |
daeyeon001@vip.163.com | China | 2062 | 58 |
Career Henan Chemica Co | +86-0371-86658258 15093356674; |
laboratory@coreychem.com | China | 30255 | 58 |
Shanxi Xuanran Import and Export Trade Co., Ltd. | +8617735180244 |
mike_yan@xuanranglobal.com | CHINA | 4022 | 58 |
Zhengzhou Anhuida Chemical Co., Ltd | +8615903659408 |
admin@ahdchem.com | China | 298 | 58 |
Jilin Chinese Academy of Sciences-yanshen Technology | +undefined18143011203 |
info@chemextension.com | China | 42057 | 58 |
Aladdin Scientific | +1-833-552-7181 |
sales@aladdinsci.com | United States | 57511 | 58 |
Henan Alfachem Co.,Ltd. | 0371-0371-55051623 18137891487 |
2853979817@qq.com | China | 9968 | 58 |
2,3,6,7,14,15-Hexabromo-9,10-dihydro-9,10-[1,2]benzenoanthracene 관련 검색:
9,10[1',2']-Benzenoanthracene-2,7,14-triamine, 9,10-dihydro-
9,10[1',2']-Benzenoanthracene-9,10-dicarboxylic acid
9,10[1',2']-Benzenoanthracene, 2,3,6,7,14,15-hexaethynyl-9,10-dihydro-
9,10-[1,2]benzenoanthracene-2,3,6,7,14,15(9H,10H)-hexaone
2,6,14-trioltriptycene
2,6,14-tribromotriptycene
2,3,6,7,14,15-Hexaaminotriptycene hexahydrochloride
2,6,14-triaminotriptycene
2,6,14-triiodotriptycene