N-Pivaloyl-L-tyrosine

N-Pivaloyl-L-tyrosine 구조식 이미지
카스 번호:
33019-85-1
상품명:
N-Pivaloyl-L-tyrosine
동의어(영문):
N-Pivaloyl-L-;Tyrosine Impurity 12;N-Pivaloyl-L-tyrosine;N-(2,2-Dimethyl-1-oxopropyl)-L-tyrosine;L-Tyrosine, N-(2,2-diMethyl-1-oxopropyl)-;(S)-3-(4-hydroxyphenyl)-2-pivalamidopropanoic acid;(2S)-2-(2,2-dimethylpropanoylamino)-3-(4-hydroxyphenyl)propanoic acid
CBNumber:
CB62545493
분자식:
C14H19NO4
포뮬러 무게:
265.3
MOL 파일:
33019-85-1.mol

N-Pivaloyl-L-tyrosine 속성

녹는점
>58°C (dec.)
저장 조건
Hygroscopic, Refrigerator, under inert atmosphere
용해도
클로로포름(약간 용해됨), DMSO(약간 용해됨), 메탄올(약간 용해됨), 물(약간 용해됨)
물리적 상태
고체
물리적 상태
단단한 모양
색상
흰색에서 옅은 베이지까지
안정성
흡습성

안전

N-Pivaloyl-L-tyrosine C화학적 특성, 용도, 생산

용도

N-Pivaloyl-L-tyrosine can be used in peptide N-terminal amino acid determination.

제조 방법

Preparation of N-Pivaloyl-L-tyrosine Ethyl Ester
N-Pivaloyl-L-tyrosine could not be prepared from L-tyrosine following the previous method. Under the same conditions used for the preparation of IK, 90% of the starting material remained unreacted. N-Pivaloyl-L-tyrosine Ethyl Ester was, however, made from Ie by mild hydrolysis with dilute sodium hydroxide solution and subsequent esterification with absolute ethyl alcohol saturated with dry HCl gas. The material after chromatography on florisil was obtained as an oil. Comparison of the mobility with Ie on thin-layer chromatography in two solvent systems (I and 11) as well as conversion to Ie by further acylation confirmed the identity of the material.

N-Pivaloyl-L-tyrosine 준비 용품 및 원자재

원자재

준비 용품


N-Pivaloyl-L-tyrosine 공급 업체

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