2-(2-chlorophenyl)cyclohexanone
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2-(2-chlorophenyl)cyclohexanone 속성
- 녹는점
- 60-62 °C
- 끓는 점
- 308.8±42.0 °C(Predicted)
- 밀도
- 1.165±0.06 g/cm3(Predicted)
- 물리적 상태
- 가루
- 색상
- 백색 결정체
- InChI
- InChI=1S/C12H13ClO/c13-11-7-3-1-5-9(11)10-6-2-4-8-12(10)14/h1,3,5,7,10H,2,4,6,8H2
- InChIKey
- UOEXWLLNMGAJDD-UHFFFAOYSA-N
- SMILES
- C1(=O)CCCCC1C1=CC=CC=C1Cl
안전
2-(2-chlorophenyl)cyclohexanone C화학적 특성, 용도, 생산
화학적 성질
white crystalline powder.용도
2-(2-Chlorophenyl)-cyclohexanone is a reactant that is used in the preparation of benzofurans via palladium-phosphine-catalyzed intramolecular enolate O-arylation of α-arylketones.Synthesis
To a flame dried flask was added Cs2CO3 (6.5 g, 20 mmol), Pd2(dba)3 (184 mg, 0.2 mmol) and Xantphos (139 mmol, 0.24 mmol). After purging with N2, toluene (10 mL), ketone (15 mmol) and phenyl iodide (1.11 mL, 10 mmol) were added. After stirring overnight at 80 .MALE.C, the mixture was filtered and concentrated in vacuo to afford a residue, which was purified by flash chromatography to provide the desired 2-(2-chlorophenyl)cyclohexanone.
2-(2-chlorophenyl)cyclohexanone 준비 용품 및 원자재
원자재
Benzene, 1-chloro-2-(2-nitrocyclohexyl)-
1-chloro-2-[(E)-2-nitroethenyl]benzene
사이클로헥센옥사이드
2-브로모클로로벤젠
사이클로헥사논
준비 용품
2-(2-chlorophenyl)cyclohexanone 공급 업체
글로벌( 89)공급 업체
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