Tetrafluoro-1-propanol manufacturers and suppliers

Tetrafluoro-1-propanol suppliers

Properties

Melting point:: -15°C

Boiling point:: 109 °C

Density: 1.48 g/mL at 20 °C(lit.)

refractive index: n20/D 1.321(lit.)

Flash point:: 110 °F

storage temp.: Sealed in dry,2-8°C

form: Liquid

pka: 13.05±0.10(Predicted)

Specific Gravity: 1.481.471

color: Clear colorless

Water Solubility: Soluble in water.

Merck: 14,9206

BRN: 1738264

Stability:: Stable. Flammable. Incompatible with strong oxidizing agents, strong bases, sodium, potassium, acid chlorides, acid anhydrides.

Safety Information

Symbol(GHS): GHS02,GHS06

Signal word: Danger

Hazard statements: H226-H319-H331

Precautionary statements: P210-P304+P340+P311-P305+P351+P338

Hazard Codes: Xn,F,Xi

Risk Statements: 10-20-36-36/37/38

Safety Statements: 26-37/39-16-36/37-36

RIDADR: UN 1986 3/PG 3

WGK Germany: 1

RTECS: UB9400000

Hazard Note: Flammable

TSCA: T

HazardClass: 3

PackingGroup: III

HS Code: 29051990

Use

Tetrafluoro-1-propanol (450mL) is added to a solution of 2.25g of NaHSO3 in 90mL of water, shaken vigorously and set aside for 24hours. The fraction distilling at or above 99o is refluxed for 4hours with 5-6g of KOH and rapidly distilled, followed by a final fractional distillation. [Kosower & Wu J Am Chem Soc 83 3142 1961.] Alternatively, shake the alcohol with alumina for 24hours, dry it overnight with anhydrous K2CO3 and distil it, taking the middle fraction (b 107-108o). [Beilstein 1 IV 2438.]

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