| 993-13-5 Basic information More.. |
Product Name: | METHYLPHOSPHONIC ACID | Synonyms: | Phosphonic acid, methyl-;METHYLPHOSPHONIC ACID;Methylphosphonicacid,98%;Methanephosphonic acid,98%;Methylphosphonic acid ,97.5%;Methanephosphonic acid, 98% 25GR;Methanephosphonic acid, 98% 5GR;NSC 119358 | CAS: | 993-13-5 | MF: | CH5O3P | MW: | 96.02 | EINECS: | 213-607-2 | Mol File: | 993-13-5.mol | |
Use
Methylphosphonic acid [993-13-5] M 96.0, m 104-106o, 105-107o, 108o, pK 1 2.12, pK 2 7.29. If it tests for Cl-, then add H2O and evaporate to dryness, repeat several times till free from Cl-. The residue solidifies to a wax-like solid. Alternatively, dissolve the acid in the minimum volume of H2O, add charcoal, warm, filter and evaporate to dryness in a vacuum over P2O5. [Kosolapoff J Am Chem Soc 75 3379 1953.] The di-Na salt is prepared from 24g of acid in 50mL of dry EtOH, and a solution of 23g Na dissolved in 400mL EtOH is added. A white precipitate is formed, but the mixture is refluxed for 30minutes to complete the reaction. Filter off the solid and recrystallise it from 50% EtOH. Dry the crystals in a vacuum desiccator. [Thompson J Chem Soc 3292 1952, Beilstein 4 IV 3498.]
- METHYLPHOSPHONIC ACID
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- US $1.00 / g
- 2021-01-06
- CAS:993-13-5
- Min. Order: 1g
- Purity: 98%
- Supply Ability: 1ton
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993-13-5
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