- 1,4-Diacetylbenzene
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- $0.00 / 10g
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2022-09-01
- CAS:1009-61-6
- Min. Order: 10g
- Purity: 98%
- Supply Ability: 10kg
- 1,4-DIACETYLBENZENE
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- $15.00 / 1KG
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2021-08-12
- CAS:1009-61-6
- Min. Order: 1KG
- Purity: 99%+ HPLC
- Supply Ability: Monthly supply of 1 ton
- 1,4-Diacetylbenzene
-
- $15.00 / 1KG
-
2021-07-02
- CAS:1009-61-6
- Min. Order: 1KG
- Purity: 99%+ HPLC
- Supply Ability: Monthly supply of 1 ton
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| 1,4-Diacetylbenzene Basic information |
| 1,4-Diacetylbenzene Chemical Properties |
| 1,4-Diacetylbenzene Usage And Synthesis |
Chemical Properties | ALMOST WHITE TO LIGHT BROWN CRYSTALLINE POWDER | Uses | 1,1''-(1,4-phenylene)bis-Ethanone can undergo oxidative C-C Bond Cleavage to synthesize an aryl carboxylic acid with an iodine catalyst . 1,1''-(1,4-phenylene)bis-Ethanone is also capable of Suzuki-Miyaura coupling. | Synthesis Reference(s) | The Journal of Organic Chemistry, 26, p. 4308, 1961 DOI: 10.1021/jo01069a031 Synthetic Communications, 26, p. 3175, 1996 DOI: 10.1080/00397919608004626 | Purification Methods | Crystallise it from EtOH (m 114o) or *benzene and dry it in a vacuum over CaCl2. Also purify it by dissolving it in acetone, treating with Norit, evaporating and recrystallising from MeOH. The dioxime has m 248-259o. [Wagner et al. J Am Chem Soc 108 7727 1986]. [Beilstein 7 H 686, 7 II 624, 7 III 3504, 7 IV 2156.] |
| 1,4-Diacetylbenzene Preparation Products And Raw materials |
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