2-ETHYL CAPRONITRILE

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Company Name: Amadis Chemical Company Limited
Tel: 0086-571-89925085
Email: sales@amadischem.com
Products Intro: Product Name:2-Ethylhexanenitrile
CAS:4528-39-6
Purity:0.97 Package:mgs,gs,kgs Remarks:A826760
Company Name: HONEST JOY HOLDINGS LIMITED  
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Company Name: 3B Scientific Corporation  
Tel: 847.281.9822
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Company Name: MDP ChemControl Ltd.  
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2-ETHYL CAPRONITRILE Basic information
Product Name:2-ETHYL CAPRONITRILE
Synonyms:2-ETHYL CAPRONITRILE;2-Ethylhexanonitrile;NSC44904;Hexanenitrile, 2-ethyl-
CAS:4528-39-6
MF:C8H15N
MW:125.21
EINECS:
Product Categories:
Mol File:4528-39-6.mol
2-ETHYL CAPRONITRILE Structure
2-ETHYL CAPRONITRILE Chemical Properties
Safety Information
MSDS Information
2-ETHYL CAPRONITRILE Usage And Synthesis
PreparationIn a 1-L round-bottomed flask, fitted with an efficient reflux condenser, were placed 2-ethylhexaneamide 1455 (286 g, 2 mol), dry benzene (300 mL), and thionyl chloride (357 g, 218 mL, 3 mol). The flask was placed in a water bath, which was quickly heated to 75–80 C° and maintained at that temperature for 4.5 h. The reaction mixture was then transferred to a 1.5-L beaker and cooled in an ice bath. A mixture of crushed ice (100 g) and water (100 mL) was added to decompose the excess thionyl chloride. Cold 50% aq. potassium hydroxide solution was then added in small portions with stirring until the mixture was alkaline to litmus. The basified mixture was then transferred to a separatory funnel, and the layers were separated. The aqueous portion was extracted with benzene (100 mL). The benzene solutions were combined and washed with 1% sodium carbonate solution (150 mL) and water (2 × 150 mL). The mixture was distilled from a modified Claisen flask, the bulk of the solvent being removed at atmospheric pressure. The yield of nitrile 1456 was 215–236 g (86–94%); bp 118–120 C°/100 mmHg.
2-ETHYL CAPRONITRILE Preparation Products And Raw materials
Tag:2-ETHYL CAPRONITRILE(4528-39-6) Related Product Information
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