- 4-Fluorobenzhydrazide
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- $1.00 / 1KG
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2019-07-06
- CAS:456-06-4
- Min. Order: 1G
- Purity: 99%
- Supply Ability: 100KG
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| | 4-Fluorobenzhydrazide Chemical Properties |
| Melting point | 162-166 °C (lit.) | | density | 1.272±0.06 g/cm3(Predicted) | | storage temp. | Keep in dark place,Sealed in dry,Room Temperature | | solubility | Soluble in methanol. | | form | Crystalline Powder | | pka | 12.17±0.10(Predicted) | | color | Orange to light brown | | CAS DataBase Reference | 456-06-4(CAS DataBase Reference) |
| Hazard Codes | Xi | | Risk Statements | 36/37/38 | | Safety Statements | 26-36 | | WGK Germany | 3 | | RTECS | DH1310000 | | HazardClass | IRRITANT | | HS Code | 29280000 |
| | 4-Fluorobenzhydrazide Usage And Synthesis |
| preparation | The synthesized ester (12.5ml) was taken into a round bottom flask (250ml), 50ml of absolute ethanol & 37.5ml of hydrazine hydrate was added in the flask. The ester, ethanol & hydrazine hydrate for the synthesis of hydrazide must be in following ratio: Ester: Absolute ethanol: Hydrazine hydrate 1 : 4 : 3 Then round bottom flask was covered with aluminium foil, placed on hot plate & allowed to stir it for almost 12-15 hrs. As the solid product appeared, reaction completion was checked by performing TLC using n-hexane, ethyl acetate & TLC cards & observed under UV lamp. After completion of reaction n-hexane was added. Solution filtered as needle like crystals appeared. Allowed it to dry & a shiny off white product was obtained that was hydrazide & product was calculated (79%).
| | Chemical Properties | White solid | | Uses | Used in the stnthesis of fluorinated poly (1, 3, 4-oxadiazole-ether-imide). N-(3,5-dinitrobenzoyl)-N?-(4-fluorobenzoyl)-hydrazine with 4-Fluorobenzhydrazide as solvent in NMP. |
| | 4-Fluorobenzhydrazide Preparation Products And Raw materials |
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