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Product Name:2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane
CAS:1822310-41-7
Purity:99% Package:1kg, 5kg, 20kg, at customer's requirement Remarks:oled materials
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| | 2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane Basic information |
| Product Name: | 2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane | | Synonyms: | 2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane;1-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)dibenzofuran;Dibenzofuran, 1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-;2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolan;Pinalol dibenzofuran-1-borate | | CAS: | 1822310-41-7 | | MF: | C18H19BO3 | | MW: | 294.15 | | EINECS: | | | Product Categories: | | | Mol File: | 1822310-41-7.mol | ![2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane Structure](CAS/20180527/GIF/1822310-41-7.gif) |
| | 2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane Chemical Properties |
| Boiling point | 427.2±18.0 °C(Predicted) | | density | 1.15±0.1 g/cm3(Predicted) | | InChI | InChI=1S/C18H19BO3/c1-17(2)18(3,4)22-19(21-17)13-9-7-11-15-16(13)12-8-5-6-10-14(12)20-15/h5-11H,1-4H3 | | InChIKey | CKQXGVLPVWNAIS-UHFFFAOYSA-N | | SMILES | O1C2=CC=CC=C2C2=C(B3OC(C)(C)C(C)(C)O3)C=CC=C12 |
| | 2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane Usage And Synthesis |
| Chemical Properties | light yellow liquid | | Uses | 2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane is a luminescent material that can be used in the composition of organic electroluminescent compounds, organic photovoltaic devices and display devices. | | Preparation | 1-bromodibenzo[b,d]furan (31.3 g, 126.7 mM), bis (pinacolato) diboron (190.0 g, 190.0 mM), PdCl2(dppf)(4.6 g, 6.3 mM), and KOAc (37.3 g, 380.1 mM) was dissolved in 300 mL of 1,4-dioxane and refluxed for 24 hours. After the reaction was completed, water and DCM (dichloromethane) were added to the mixture at room temperature. The organic layer was dried with MgSO4 and the solvent was removed by a rotary evaporator. The product was purified by column chromatography and recrystallized from methanol to obtained 2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane.
| | storage | Store at 0-8 °C |
| | 2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane Preparation Products And Raw materials |
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