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3,6-Dibromopyridazide

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CAS:17973-86-3
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CAS:17973-86-3
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CAS:17973-86-3
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3,6-Dibromopyridazide manufacturers

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  • $0.00 / 1KG
  • 2022-01-04
  • CAS:17973-86-3
  • Min. Order: 1g
  • Purity: 99%minHPLC
  • Supply Ability: 100kgs/month
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  • $1.10 / 1g
  • 2021-11-02
  • CAS:17973-86-3
  • Min. Order: 1g
  • Purity: 99.00%
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3,6-Dibromopyridazide Basic information
Product Name:3,6-Dibromopyridazide
Synonyms:3,6-Dibromopyridazine ,97%;Pyridazine, 3,6-dibromo-;3,6-dibromopyridazide;3,6-Dibromo-1,2-diazine;3,6-Dibromopyridazide ISO 9001:2015 REACH;3,6-DIBROMOPYRIDAZINE
CAS:17973-86-3
MF:C4H2Br2N2
MW:237.88
EINECS:687-847-5
Product Categories:Heterocycle-other series;Building Blocks;Pyridazine;Halides;Pyrazines, Pyrimidines & Pyridazines;Pyrazines, Pyrimidines & Pyridazines
Mol File:17973-86-3.mol
3,6-Dibromopyridazide Structure
3,6-Dibromopyridazide Chemical Properties
Melting point 116 °C
Boiling point 327.5±22.0 °C(Predicted)
density 2?+-.0.06 g/cm3(Predicted)
storage temp. Keep in dark place,Sealed in dry,Room Temperature
pka-1.18±0.10(Predicted)
form Solid
color White to pale yellow
InChIInChI=1S/C4H2Br2N2/c5-3-1-2-4(6)8-7-3/h1-2H
InChIKeyVQAFMTSSCUETHA-UHFFFAOYSA-N
SMILESC1(Br)=NN=C(Br)C=C1
Safety Information
Hazard Codes Xn
Risk Statements 36/37/38-20/21/22-22
Safety Statements 26-36/37/39-22-37/39-36/37-24/25
WGK Germany 3
Hazard Note Harmful
HS Code 29339900
MSDS Information
3,6-Dibromopyridazide Usage And Synthesis
Chemical PropertiesGrey yellow powder
Uses3,6-dibromopyridazine is an important intermediate in organic synthesis. It is mainly used in pharmaceutical intermediates, organic synthesis, organic solvents, and can also be used in dye production, pesticide production and perfumery.
Preparation3,6-dibromopyridazine for Synthesis: A mixture of maleic hydrazide (1.1 g, 10 mmol) and PBr5 (4.7 g, 11 mmol) was heated at 100 °C until no more white fumes of hydrogen bromide were produced (~2 h). After cooling, the orange residue was poured into ice water and the resulting mixture was extracted with CH2Cl2 (3 x 20 mL). The organic layer was washed with saturated aqueous NaHCO3, dried over MgSO4, filtered and concentrated. The crude product was purified by flash column chromatography on silica gel (CH2Cl2) to give 3,6-dibromopyridazine as a white solid (1.20 g, 50%).
Tag:3,6-Dibromopyridazide(17973-86-3) Related Product Information
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