- THIOFORMAMIDE
-
- $1.00 / 1KG
-
2020-01-08
- CAS:115-08-2
- Min. Order: 100KG
- Purity: 98%-99.9%
- Supply Ability: 200KG
|
| | THIOFORMAMIDE Basic information |
| Product Name: | THIOFORMAMIDE | | Synonyms: | THIOFORMAMIDE;Aminomethanethione;Formthioamide;Einecs 204-063-7;Thioformamide (40-50% w/w in THF);Methanethioamide (9CI);Methanethioamide;"THIOFORMAMIDE Methanethioamide" | | CAS: | 115-08-2 | | MF: | CH3NS | | MW: | 61.11 | | EINECS: | 204-063-7 | | Product Categories: | | | Mol File: | 115-08-2.mol |  |
| | THIOFORMAMIDE Chemical Properties |
| Melting point | 28-29℃ | | Boiling point | 105℃ | | density | 1.133 | | Fp | 17℃ | | solubility | DMSO (Sparingly), THF (Soluble) | | form | Colourless to Dark Brown Solution | | pka | 12.60±0.29(Predicted) |
| | THIOFORMAMIDE Usage And Synthesis |
| Uses | Thioformamide, can be used in the synthesis of sulfoximine tethered heterocycles used as key building blocks. | | Purification Methods | Crystallise thioformamide from EtOAc, Et2O or ether/pet ether. The monohydrate is a yellow oil soluble in many organic solvents. UV: 263nm ( 2500) in MeOH. [Erlenmyer & Menzi Helv Chim Acta 31 2071 1948.] Alternatively dissolve it in Et2O to separate it from any formanide and/or polymers, filter, evaporate and recrystallise the residue from EtOAc at Dry-Ice temperature [Londergan et al. J Am Chem Soc 75 4456 1953]. Store it in Et2O solution over P2O5. [Cousineau & Secrist J Org Chem 44 4351 1979, Beilstein 2 H 95, 2 I 39, 2 III 128, 2 IV 92.] |
| | THIOFORMAMIDE Preparation Products And Raw materials |
|