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Levulinic acid

Levulinic acid Suppliers list
Company Name: Henan Tianfu Chemical Co.,Ltd.
Tel: 0371-55170693
Email: info@tianfuchem.com
Products Intro: CAS:123-76-2
Purity:99% Package:500G;1KG;5KG;25KG
Company Name: Capot Chemical Co.,Ltd.
Tel: +86 (0)571-855 867 18
Email: sales@capotchem.com
Products Intro: Product Name:Levulinic acid
CAS:123-76-2
Purity:98%(min,HPLC) Package:100g;1kg;5kg,10kg,25kg,50kg
Company Name: Shenzhen Sendi Biotechnology Co.Ltd.
Tel: 0755-23311925 18102838259
Email: Abel@chembj.com
Products Intro: Product Name:Levulinic acid
CAS:123-76-2
Purity:99% Package:26/KG
Company Name: Henan DaKen Chemical CO.,LTD.
Tel: +86-371-55531817
Email: info@dakenchem.com
Products Intro: Product Name:Levulinic acid
CAS:123-76-2
Purity:99% Package:100g,500g,1kg,5kg,10kg
Company Name: Mainchem Co., Ltd.
Tel: +86-0592-6210733
Email: sales@mainchem.com
Products Intro: Product Name:Levulinic acid
CAS:123-76-2

Lastest Price from Levulinic acid manufacturers

  • Levulinic acid
  • US $8450.00 / KG
  • 2018-07-24
  • CAS:123-76-2
  • Min. Order: 200KG
  • Purity: 99%
  • Supply Ability: 100tons
Levulinic acid Basic information
Content analysis Physicochemical Properties Application Preparation Toxicity Usage limit
Product Name:Levulinic acid
Synonyms:3-acetyl-propionicaci;3-Keto-n-velericacid;4-Keto-n-valericacid;4-Oxo-pentanoic acid (levulinic acid);4-oxo-pentanoicaci;4-oxovaleric;4-oxo-valericaci;4-Oxpentanoicacid
CAS:123-76-2
MF:C5H8O3
MW:116.12
EINECS:204-649-2
Product Categories:Fatty & Aliphatic Acids, Esters, Alcohols & Derivatives;Biochemistry;Reagents for Oligosaccharide Synthesis;Dextrins、Sugar & Carbohydrates;Building Blocks;C1 to C5;Carbonyl Compounds;Carboxylic Acids;Chemical Synthesis;Organic Building Blocks;Pharma material;ACETYLGROUP;Intermediates
Mol File:123-76-2.mol
Levulinic acid Structure
Levulinic acid Chemical Properties
Melting point 30-33 °C(lit.)
Boiling point 245-246 °C(lit.)
density 1.134 g/mL at 25 °C(lit.)
vapor pressure 1 mm Hg ( 102 °C)
refractive index n20/D 1.439(lit.)
FEMA 2627 | LEVULINIC ACID
Fp 280 °F
storage temp. Store below +30°C.
solubility 675g/l
form Liquid After Melting
pkapKa 4.65(H2O,t = 25,c=0.03-0.001) (Uncertain)
color Clear yellow
Water Solubility Soluble in water ( 675g/L at 20°C).
Sensitive Light Sensitive
Merck 14,5472
BRN 506796
InChIKeyJOOXCMJARBKPKM-UHFFFAOYSA-N
CAS DataBase Reference123-76-2(CAS DataBase Reference)
NIST Chemistry ReferencePentanoic acid, 4-oxo-(123-76-2)
EPA Substance Registry SystemPentanoic acid, 4-oxo-(123-76-2)
Safety Information
Hazard Codes Xn,C
Risk Statements 22-36/37/38-34-R34-R22
Safety Statements 26-45-36/37/39-S45-S36/37/39-S26
RIDADR 3261
WGK Germany 3
RTECS OI1575000
TSCA Yes
HazardClass 8
PackingGroup III
HS Code 29183000
ToxicityLD50 orally in Rabbit: 1850 mg/kg LD50 dermal Rabbit > 5000 mg/kg
MSDS Information
ProviderLanguage
Levulic acid English
ACROS English
SigmaAldrich English
ALFA English
Levulinic acid Usage And Synthesis
Content analysisAccurately weigh about 1.0 g of the sample, and put it into a 250ml Erlenmeyer flask containing 75~100ml water, add phenolphthalein test solution; apply 0.5 mol/L sodium hydroxide for titration to until it began to appear pink and maintain 15 s. Each mL of 0.5mol/L sodium hydroxide solution is equivalent to 58.08mg of the goods.
Physicochemical PropertiesWhite flake crystals, hygroscopic. It is easily soluble in water and alcohol, ether organic solvents.
ApplicationIt can be used as the raw materials of medicine, spices and paint, and used as solvent.
This product has wide applications. Levulinic acid can be used as both a carboxylic acid and can also be used as a ketone for reaction for making various kinds of products through esterification, halogenation, hydrogenation, oxidation dehydrogenation, condensation, etc., including resins, pharmaceuticals, spices, solvents, rubber and plastic additives, lubricants additives, surfactants and so on. In the pharmaceutical industry, its calcium salt (calcium fructose) can be used for intravenous injection. As a nutritional medicine, it helps to boost the formation of bone and maintain the normal excitability of nerves and muscles. It can also used for the production of indomethacin and plant hormones. Levulinic acid manufactured bisphenol acid can be made of water-soluble resin, used in the paper industry to produce filter paper. Levulinic acid is also an intermediate of pesticides and dyes.
Used for biochemical reagents, but also for organic synthesis
It can be used as an important chemical raw material or solvents. It can be used for the manufacturing of medicine (intravenous injection, indomethacin, etc.), resin (bisphenol acid water-soluble resin), spices (spices or tobacco spices), paint, paint, pesticides, and surfactants.
It can be used for biochemical research; manufacturing of esters and drugs. It is also the inhibitor of chlorophyll synthesis.
PreparationThe residue during the manufacturing of furfural with cotton seed shell or corncob sugar (furfural residue) or waste taro residue, through pressured hydrolysis with dilute acid, can be used to produce levulinic acid. The furfural residue was added to 10% dilute hydrochloric acid, the solidified solution was 1: 1.75, mixed and put into the hydrolysis pot, steamed at a pressure of 0.2MPa for 8-10 h. The diluted solution is then filtered and concentrated to a concentration of about 50%. It is further subject to vacuum distillation for collecting the fraction above 130 ℃ (2.67kPa) to obtain the finished product. Raw material consumption quota: potato tacar 7,000 kg/t, hydrochloric acid (fold 100%) 1800kg/t. Another method is manufacturing through the rearrangement and hydrolysis of sugar alcohol.
4% hydrochloric acid solution was added to the reaction pot, stir and heat to 97-100 ℃, slowly add the mixture of furfuryl alcohol, ethanol and water. After addition, stir 30 min. The filtrate was concentrated at 80 ° C (21.3 kPa) under reduced pressure to give crude levulinic acid. Then apply vacuum distillation, collect the fraction of 160-170 ° C (2.67kPa), and then re-distill once, to obtain the refined levulinic acid with the yield of about 75%.
ToxicityGRAS (FEMA).
Usage limitFEMA (mg/kg): Beverage, cold drink, 14.0; Candy, baked goods, 53.0; Gelatin, pudding, 4.0.
FDA, §172.515 (2000): take proper amount as limit.
Chemical Propertiesclear yellowish liquid after melting
UsesReplenisher (calcium).
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