Company Name: |
Shanghai Hong-chuang Pharma Tech Co., Ltd.
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Tel: |
18151128828 |
Email: |
hc-sales@foxmail.com |
Products Intro: |
Product Name:1-Methoxy-2-phenylethaniMiniuM chloride CAS:39496-45-2 Purity:97% Package:1g,5g,25g,100g,250g,500g,1kg
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Company Name: |
Chengdu J&B Technology Co., Ltd.
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Tel: |
28-61186694 15608078506 |
Email: |
598677760@qq.com |
Products Intro: |
Product Name: 1-Methoxy-2-phenylethaniMiniuM chloride CAS:39496-45-2 Purity:97% Package:5g/RMB 6900;50g
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Company Name: |
Changzhou Hopschain Chemical Co.,Ltd.
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Tel: |
0519-85528066 13775048983 |
Email: |
sales@hopschem.com |
Products Intro: |
Product Name:1-methoxy-2-phenylethaniminium chloride CAS:39496-45-2 Purity:97+% Package:1g;5g
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Company Name: |
Cool Pharm, Ltd
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Tel: |
18019463053 |
Email: |
sales@coolpharm.com |
Products Intro: |
Product Name:Methyl2-phenylacetimidatehydrochloride CAS:39496-45-2 Purity:95.0% Package:10g;25g;100g;500g;1kg;5kg;10kg
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| 1-Methoxy-2-phenylethaniMiniuM chloride Basic information |
| 1-Methoxy-2-phenylethaniMiniuM chloride Chemical Properties |
| 1-Methoxy-2-phenylethaniMiniuM chloride Usage And Synthesis |
Preparation | To a 50-ml pear-shaped flask equipped with a water-reflux condenser, a gas inlet tube reaching the bottom of the flask, and a gas outlet tube fitted with a drying tube is added 2.85 ml (2.90 g, 24.7 mmol) of phenylacetonit-rile, 1.00 ml of dry methanol (0.80 g, 24.7 mmol) and 7 ml of anhydrous ether. The flask is cooled in an ice bath while dry hydrogen chloride gas (first passed through sulfuric acid) is passed into the solution until no more was absorbed.The flask is then disconnected, stoppered tightly, and stored at -10°C overnight. A solid forms, which is isolated by filtration under a stream of argon gas and then dried under reduced pressure for 4 hrs, to yield 4.30 g (23.2 mmol or 94% yield) of a white free-flowing powder. The NMR (CDCI3, 90MHz) indicated 7.32 (m, 5H), 4.23 (s, 3H), 4.05 (s, 2H).
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| 1-Methoxy-2-phenylethaniMiniuM chloride Preparation Products And Raw materials |
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