1-Methoxy-2-phenylethaniMiniuM chloride

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Products Intro: Product Name:methyl 2-phenylethanimidate,hydrochloride
CAS:39496-45-2
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Products Intro: Product Name:1-Methoxy-2-phenylethaniMiniuM chloride
CAS:39496-45-2
Purity:97% Package:1g,5g,25g,100g,250g,500g,1kg
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Products Intro: Product Name: 1-Methoxy-2-phenylethaniMiniuM chloride
CAS:39496-45-2
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Products Intro: Product Name:1-methoxy-2-phenylethaniminium chloride
CAS:39496-45-2
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Products Intro: Product Name:Methyl2-phenylacetimidatehydrochloride
CAS:39496-45-2
Purity:95.0% Package:10g;25g;100g;500g;1kg;5kg;10kg
1-Methoxy-2-phenylethaniMiniuM chloride Basic information
Product Name:1-Methoxy-2-phenylethaniMiniuM chloride
Synonyms:1-Methoxy-2-phenylethaniMiniuM chloride;methyl 2-phenylacetimidate hydrochloride;methyl 2-phenylethanimidate,hydrochloride;METHYL PHENYLACETIMIDATE HYDROCHLORIDE
CAS:39496-45-2
MF:C9H12ClNO
MW:185.65068
EINECS:
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Mol File:39496-45-2.mol
1-Methoxy-2-phenylethaniMiniuM chloride Structure
1-Methoxy-2-phenylethaniMiniuM chloride Chemical Properties
Safety Information
MSDS Information
1-Methoxy-2-phenylethaniMiniuM chloride Usage And Synthesis
PreparationTo a 50-ml pear-shaped flask equipped with a water-reflux condenser, a gas inlet tube reaching the bottom of the flask, and a gas outlet tube fitted with a drying tube is added 2.85 ml (2.90 g, 24.7 mmol) of phenylacetonit-rile, 1.00 ml of dry methanol (0.80 g, 24.7 mmol) and 7 ml of anhydrous ether. The flask is cooled in an ice bath while dry hydrogen chloride gas (first passed through sulfuric acid) is passed into the solution until no more was absorbed.The flask is then disconnected, stoppered tightly, and stored at -10°C overnight. A solid forms, which is isolated by filtration under a stream of argon gas and then dried under reduced pressure for 4 hrs, to yield 4.30 g (23.2 mmol or 94% yield) of a white free-flowing powder. The NMR (CDCI3, 90MHz) indicated 7.32 (m, 5H), 4.23 (s, 3H), 4.05 (s, 2H).
Preparation of Methyl Phenylacetimidate Hydrochloride
1-Methoxy-2-phenylethaniMiniuM chloride Preparation Products And Raw materials
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