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DIBUTYLCARBAMYL CHLORIDE

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Company Name: CONIER CHEM AND PHARMA LIMITED
Tel: 86-18523575427
Email: sales@conier.com
Products Intro: CAS:13358-73-1
Purity:0.99 Package:1kg
Company Name: Shaanxi Dideu Medichem Co. Ltd
Tel:
Email: 1010@dideu.com
Products Intro: Product Name:DIBUTYLCARBAMYL CHLORIDE ISO 9001:2015 REACH
CAS:13358-73-1
Purity:99.00% Package:25kgs/Drum;200kgs/Drum Remarks:ISO 9001:2015 REACH Approved Manufacturer
Company Name: Shaanxi Dideu Medichem Co. Ltd
Tel:
Email: 1015@dideu.com
Products Intro: Product Name:Dibutylcarbamyl chloride
CAS:13358-73-1
Purity:99.0%+ Package:1KG;USD|20KG;USD|25KG;USD
Company Name: Hefei TNJ Chemical Industry Co.,Ltd.
Tel: 0551-65418671
Email: sales@tnjchem.com
Products Intro: Product Name:Dibutylcarbamyl Chloride
CAS:13358-73-1
Company Name: Meryer (Shanghai) Chemical Technology Co., Ltd.  
Tel: 21-61259100-
Email: sh@meryer.com
Products Intro: Product Name:DibutylcarbaMic chloride
CAS:13358-73-1
Purity:98% Package:500g Remarks:C51165

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DIBUTYLCARBAMYL CHLORIDE Basic information
Product Name:DIBUTYLCARBAMYL CHLORIDE
Synonyms:DIBUTYLCARBAMYL CHLORIDE;1,6-dibutyl-carbamicchlorid;dibutyl-carbamoylchlorid;dibutylcarbamoylchloride;tl459;N,N-dibutylcarbamoyl chloride;Dibutylcarbamic acid chloride;Brn 2040828
CAS:13358-73-1
MF:C9H18ClNO
MW:191.7
EINECS:236-410-3
Product Categories:Acid Halides;Carbonyl Compounds;Organic Building Blocks
Mol File:13358-73-1.mol
DIBUTYLCARBAMYL CHLORIDE Structure
DIBUTYLCARBAMYL CHLORIDE Chemical Properties
Boiling point 257-260 °C(lit.)
density 0.985 g/mL at 25 °C(lit.)
refractive index n20/D 1.456(lit.)
Fp 110 °C
pka-1.85±0.70(Predicted)
Safety Information
Hazard Codes C
Risk Statements 34
Safety Statements 26-36/37/39-45
RIDADR UN 3265 8/PG 3
WGK Germany 3
RTECS FD2230000
HazardClass IRRITANT
MSDS Information
ProviderLanguage
SigmaAldrich English
DIBUTYLCARBAMYL CHLORIDE Usage And Synthesis
PreparationIn a 100 mL roundbottomed flask were placed dibutylamine (6.45 g, 0.05 mol), pyridine (4.0 g, 0.05 mol), N-cyclohexyl-N0,N0,N00,N00-tetraethylguanidine (12.7 g, 0.05 mol), and toluene (40 mL). The resulting solution was cooled to 10 °C using an ice/salt bath and carbon dioxide was bubbled into the cooled solution for 30 min. After this period of time, the pre-formed carbamate solution was added in a single portion via a cannula to a cooled ( 10 °C) solution of thionyl chloride (6 g, 0.05 mol) in toluene (40 mL). The reaction mixture was stirred at 10 °C for 45 min. It was then poured into 0.1 m aq. HCl (100 mL), giving rise to two layers. The organic layer was separated, dried over anhydrous Mg2SO4, filtered, and the solvent was removed in vacuo. The residue was distilled in vacuo (1 mmHg) at 95–98 °C to give 7.62 g (79%) of N,N-dibutyl carbamoyl chloride.
DIBUTYLCARBAMYL CHLORIDE Preparation Products And Raw materials
Tag:DIBUTYLCARBAMYL CHLORIDE(13358-73-1) Related Product Information
N,N-DI-N-PROPYLFORMAMIDE Diethylcarbamyl chloride carbamoyl chloride N,N-Dibutylformamide DIBUTYLAMINE HYDROCHLORIDE DIBUTYLCARBAMYL CHLORIDE Ethylmethyl-carbamic chloride Dimethylcarbamoyl chloride DIMETHYLFORMAMIDE HYDROGEN CHLORIDE COMPLEX