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p-Nitrobenzamide

p-Nitrobenzamide Basic information
Product Name:p-Nitrobenzamide
Synonyms:p-nitro-benzamid;P-NITROBENZAMIDE;TIMTEC-BB SBB008201;4-Nitrobenzamide p-Nitrobenzamide;4-Nitrobenzamide>99.0%;4-NITROBENZAMIDE;4-Nitrobenzamide, 98+%;4-Carbamoylnitrobenzene
CAS:619-80-7
MF:C7H6N2O3
MW:166.13
EINECS:210-613-7
Product Categories:Pharmaceutical Intermediates;Amides;Carbonyl Compounds;Organic Building Blocks;Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts
Mol File:619-80-7.mol
p-Nitrobenzamide Structure
p-Nitrobenzamide Chemical Properties
Melting point 199-201 °C(lit.)
Boiling point 294.32°C (rough estimate)
density 1.4334 (rough estimate)
refractive index 1.5880 (estimate)
pka15.02±0.50(Predicted)
form powder to crystal
color White to Orange to Green
Water Solubility <0.01 g/100 mL at 18 ºC
BRN 639263
Stability:Stable. Incompatible with strong oxidizing agents, strong bases.
CAS DataBase Reference619-80-7(CAS DataBase Reference)
NIST Chemistry ReferenceBenzamide, 4-nitro-(619-80-7)
EPA Substance Registry Systemp-Nitrobenzamide (619-80-7)
Safety Information
Hazard Codes T,Xn
Risk Statements 23/24/25-22-20/21/22
Safety Statements 27-28-36/37/39-45-36
WGK Germany 3
RTECS CV5601000
TSCA Yes
HS Code 29242990
MSDS Information
ProviderLanguage
4-Nitrobenzamide English
SigmaAldrich English
ACROS English
ALFA English
p-Nitrobenzamide Usage And Synthesis
Chemical Propertieswhite powder
Uses4-Nitrobenzamide was used in the preparation of 4-nitrobenziminosulfurane.
Synthesis Reference(s)Tetrahedron Letters, 36, p. 3469, 1995 DOI: 10.1016/0040-4039(95)00528-K
General DescriptionWhite powder.
Air & Water ReactionsInsoluble in water.
Reactivity ProfileA nitrated amide. Organic amides/imides react with azo and diazo compounds to generate toxic gases. Flammable gases are formed by the reaction of organic amides/imides with strong reducing agents. Amides are very weak bases (weaker than water). Imides are less basic yet and in fact react with strong bases to form salts. That is, they can react as acids. Mixing amides with dehydrating agents such as P2O5 or SOCl2 generates the corresponding nitrile. The combustion of these compounds generates mixed oxides of nitrogen (NOx).
Fire HazardFlash point data for p-Nitrobenzamide are not available, however, p-Nitrobenzamide is probably combustible.
p-Nitrobenzamide Preparation Products And Raw materials
Preparation ProductsDabigatran Impurity 8-->5-(4-NITRO-PHENYL)-2H-TETRAZOLE
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