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| | 3-Methylaminopropionitrile Basic information |
| | 3-Methylaminopropionitrile Chemical Properties |
| | 3-Methylaminopropionitrile Usage And Synthesis |
| Chemical Properties | CLEAR YELLOW LIQUID | | Uses | (3-MethylaMinopropionitrile) Aminoproponitriles can be used as inhibitors of oxidase enzymes and as a reagent for aminomethylphosphine ligands or the synthesis of aminobenzothiazoles. | | Synthesis | Below 15 °C, 160.8 g (3.0 mol, 99% purity) of 2-acrylonitrile was slowly added dropwise to 345.1 g (3.0 mol, 27% concentration) of monomethylamine solution while maintaining stirring. Upon completion of the reaction, the ethanol generated was removed by distillation at atmospheric pressure. The product was subsequently collected by vacuum distillation to give 210.6 g of 3-methylaminopropionitrile in 83.5% yield. | | References | [1] Kinetics and Catalysis, 2010, vol. 51, # 5, p. 653 - 656
[2] Journal of Heterocyclic Chemistry, 1997, vol. 34, # 1, p. 87 - 91
[3] Patent: CN106632280, 2017, A. Location in patent: Paragraph 0023; 0024; 0025
[4] Patent: CN108003141, 2018, A. Location in patent: Paragraph 0032; 0035
[5] Liebigs Annalen der Chemie, 1980, # 9, p. 1438 - 1447 |
| | 3-Methylaminopropionitrile Preparation Products And Raw materials |
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