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| | 5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE Basic information |
| Product Name: | 5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE | | Synonyms: | O,O'-Benzylidenepentaerythritol
Monobenzalpentaerythritol;1,3-Dioxane-5,5-dimethanol, 2-phenyl-;2-phenyl-m-dioxane-5,5-dimethanol;2-phenyl-m-dioxane-5-dimethanol;5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE;2-PHENYL-1,3-DIOXANE-5,5-DIMETHANOL;O,O'-BENZYLIDENEPENTAERYTHRITOL;MONOBENZALPENTAERYTHRITOL | | CAS: | 2425-41-4 | | MF: | C12H16O4 | | MW: | 224.25 | | EINECS: | | | Product Categories: | Dioxanes;Dioxanes & Dioxolanes | | Mol File: | 2425-41-4.mol |  |
| | 5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE Chemical Properties |
| Melting point | 135 °C | | Boiling point | 325.65°C (rough estimate) | | density | 1.1697 (rough estimate) | | refractive index | 1.5130 (estimate) | | storage temp. | Sealed in dry,Room Temperature | | form | powder to crystal | | pka | 14.27±0.10(Predicted) | | color | White to Almost white | | InChIKey | DHWCGYXHBIWIPM-UHFFFAOYSA-N | | CAS DataBase Reference | 2425-41-4(CAS DataBase Reference) |
| RTECS | JH0300000 | | HS Code | 2932.99.7000 |
| | 5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE Usage And Synthesis |
| Preparation | To a flask containing a solution of 136.0 gm (1.0 mole) of pentaerythritol in 1 liter of water (25-29°C) is added 5.0 ml of concentrated hydrochloric acid and then 106 gm (1.0 mole) of benzaldehyde is dropwise added (approx. 2 - 3 hr). The mixture is stirred for 3-5 hr and then the precipitated product is filtered, recrystallized from 1500 ml of slightly alkaline water ( N a 2C03) , filtered, and dried. The product is again recrystallized from toluene (1.3-1.5 liters) to afford 175 gm (80%), m.p. 133.5°C.
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| | 5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE Preparation Products And Raw materials |
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