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| | 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Basic information |
| Product Name: | 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene | | Synonyms: | 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-Methylbenzene
4-(3-Acryloyloxypropyloxy)-benzoesure -2-Methyl-1, 4-phenylester;2-Methyl-1,4-phenylene-bis[4[3(acryloyloxy)propyloxy]benzoate];4-(3-Acryloyloxypropyloxy)benzoic acid 2-methyl-1,4-phenylene ester;Benzoic acid, 4-[3-[(1-oxo-2-propenyl)oxy]propoxy]-,2-methyl-1,4-phenylene ester;4- (3-acryloyloxy-propoxy) benzoic acid 2-methyl-1,4-phenylene ester;1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenze;4-(3-Acryloyloxypropyloxy)-benzoesure 2-methyl-1, 4-phenylester;Benzoic acid, 4-[3-[(1-oxo-2-propen-1-yl)oxy]propoxy]-, 1,1'-(2-methyl-1,4-phenylene) ester | | CAS: | 174063-87-7 | | MF: | C33H32O10 | | MW: | 588.6 | | EINECS: | 425-560-7 | | Product Categories: | | | Mol File: | 174063-87-7.mol | ![1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Structure](CAS/GIF/174063-87-7.gif) |
| | 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Chemical Properties |
| Boiling point | 733.5±60.0 °C(Predicted) | | density | 1.219 | | vapor pressure | 0.003Pa at 25℃ | | storage temp. | Keep in dark place,Sealed in dry,Room Temperature | | form | powder | | color | White | | Water Solubility | 5.3μg/L at 20℃ | | LogP | 5.3 at 40℃ |
| | 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Usage And Synthesis |
| Chemical Properties | White to Almost white powder to crystal | | Application | 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene is one of
numerous organic compounds composing American Elements's comprehensive
catalog of life science products. | | Flammability and Explosibility | Not classified | | Synthesis | The synthesis of 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene is as follows:Stirrer, was added methanesulfonyl chloride 5.00 g (43.6 mmol) and tetrahydrofuran 10mL the reactor having a thermometer and two dropping device. Ice-cold while each by dropping a tetrahydrofuran solution 30mL of formula tetrahydrofuran solution 60mL and triethylamine 5.25g of (I-3-1) represented by the compound 12.9g (44.1 mmol) of (51.9 mmol) from device (equation (solution of the compound represented by I-3-1)) :( triethylamine solution) = 2: were added dropwise simultaneously with one of the drip rate.After stirring for 1 hour while cooling with ice, it was added 4-dimethylaminopyridine 2.64 g (21.6 mmol) and 2- (4-hydroxyphenyl) ethanol 2.69 g (19.4 mmol).With ice-cooling was added dropwise triethylamine 5.25g (51.9 mmol).After stirring for 7 hours, the solvent was distilled off and treated added for liquid separation dichloromethane and 5% hydrochloric acid.After the organic layer was washed with brine neutralization, and purified by column chromatography (silica gel) and reprecipitated (dichloromethane / methanol) to give the compound 12.2g of formula (I-3).82% yield, had a purity of 99.63%. 
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| | 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Preparation Products And Raw materials |
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