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Methylamine hydrochloride

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CAS:593-51-1
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CAS:593-51-1
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CAS:593-51-1
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CAS:593-51-1
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CAS:593-51-1
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Methylamine hydrochloride Basic information
Product Name:Methylamine hydrochloride
Synonyms:Methylamine-hydrogenchloride(1/1);Methyl-ammonium;MERCURIALIN HYDROCHLORIDE;METHYLAMINE HYDROCHLORIDE;METHYLAMINE HCL;METHYLAMMONIUM CHLORIDE;AMINOMETHANE HYDROCHLORIDE;MONOMETHYLAMINE HCL
CAS:593-51-1
MF:CH6ClN
MW:67.52
EINECS:209-795-0
Product Categories:amine series;Amine Salts;Building Blocks;Chemical Synthesis;Nitrogen Compounds;Organic Building Blocks;NULL;Others;methylamine hydrochloride;Amine Salts;Nitrogen Compounds;Organic Building Blocks
Mol File:593-51-1.mol
Methylamine hydrochloride Structure
Methylamine hydrochloride Chemical Properties
Melting point 231-233 °C(lit.)
Boiling point 225-230 °C15 mm Hg(lit.)
density 0.8306 (rough estimate)
refractive index 1.5500 (estimate)
Fp 225-230°C/15mm
storage temp. Store below +30°C.
solubility soluble
form powder
color White crystalline
OdorOdorless
PH5-7 (10g/l, H2O, 20℃)
PH Range5 - 7 at 10 g/l at 20 °C
Water Solubility soluble
Sensitive Hygroscopic
Merck 14,6014
BRN 3588822
Stability:Stable, but may be moisture sensitive. Incompatible with strong oxidizing agents.
InChIKeyNQMRYBIKMRVZLB-UHFFFAOYSA-N
CAS DataBase Reference593-51-1(CAS DataBase Reference)
NIST Chemistry ReferenceMethylammonium chloride(593-51-1)
EPA Substance Registry SystemMethylamine hydrochloride (593-51-1)
Safety Information
Hazard Codes Xn
Risk Statements 22-36/37/38
Safety Statements 26-37/39
WGK Germany 1
RTECS PA0603000
10
TSCA Yes
HS Code 29211190
MSDS Information
ProviderLanguage
Methylammonium chloride English
ACROS English
SigmaAldrich English
ALFA English
Methylamine hydrochloride Usage And Synthesis
Chemical Propertieswhite to light tan solid
DefinitionChEBI: The hydrochloride formed from methylamine.
PreparationMethylamine hydrochloride is prepared by heating a mixture of aqueous formaldehyde and ammonium chloride; the residual water and the formic acid produced in the reaction are removed via vacuum distillation. This leaves behind solid methylamine hydrochloride. The solid is then purified by organic extractions and additional vacuum distillations. Methylamine gas for the reaction with P2P is generated in situ by heating the hydrochloride salt with sodium hydroxide. Alternatively, methylamine can be liberated from the hydrochloride with base and collected in a cold finger or flask immersed in a dry ice bath.
Purification MethodsCrystallise the salt from n-butanol, absolute EtOH or MeOH/CHCl3. Wash it with CHCl3 to remove traces of dimethylamine hydrochloride. Dry it under vacuum first with H2SO4 then P2O5. It is deliquescent; store it in a desiccator over P2O5. [Beilstein 4 IV 122.]
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