- 3'-Hydroxypropiophenone
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- $0.00 / 25kg
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2022-08-10
- CAS:13103-80-5
- Min. Order: 1kg
- Purity: 99%min
- Supply Ability: 10tons
- 3'-Hydroxypropiophenone
-
- $100.00 / 1KG
-
2019-07-06
- CAS:13103-80-5
- Min. Order: 1KG
- Purity: 99%
- Supply Ability: Customized
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| | 3'-Hydroxypropiophenone Basic information |
| Product Name: | 3'-Hydroxypropiophenone | | Synonyms: | 1-(3-hydroxyphenyl)propan-1-one;1-Propanone,1-(3-hydroxyphenyl)-;3-HYDROXY PROPIOPHENONE;3'-HYDROXYPROPIOPHENONE;Metaraminol Bitartrate Impurity 13;Ephedrine Impurity 7;3'-Hydroxypropiophenone | | CAS: | 13103-80-5 | | MF: | C9H10O2 | | MW: | 150.17 | | EINECS: | 236-027-1 | | Product Categories: | | | Mol File: | 13103-80-5.mol |  |
| | 3'-Hydroxypropiophenone Chemical Properties |
| Melting point | 82 °C | | Boiling point | 288.9±23.0 °C(Predicted) | | density | 1.104±0.06 g/cm3(Predicted) | | storage temp. | Inert atmosphere,Room Temperature | | solubility | Chloroform (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly) | | form | Solid | | pka | 9.09±0.10(Predicted) | | color | Off-White to Beige | | CAS DataBase Reference | 13103-80-5(CAS DataBase Reference) |
| | 3'-Hydroxypropiophenone Usage And Synthesis |
| Uses | 1-?(3-?Hydroxyphenyl)?-?1-?propanone is a reactant used to synthesize tricyclic fused pyridines, a family of alkaloids with antimalarial activity. | | Preparation | Preparation by diazotization of m-aminopropiophenone, followed by decomposition of the diazonium salt obtained, (71%)
Also obtained by saponification of 3-acetoxypropiophenone (b.p.2 127–128°) with refluxing 10% sodium hydroxide for 2–3 h (83%)
Also obtained by reductive deamination of 2-amino-5-hydroxypropiophenone (diazotization, followed by decomposition of the diazonium salt formed with copper powder in ethanol)
Also obtained by reaction of ethylmagnesium bromide with 3-hydroxy-N, N-diethylbenzamide in refluxing n-butyl ether for 4 h (75%)
Also obtained by treatment of 3-methoxypropiophenone (b.p.0.05 70–76°) with pyridinium chloride at 210° for 30 min (85%)
Also obtained by treatment of 1-hydroxy-1-(3-hydroxyphenyl)propane (m.p. 105–107°) with DDQ in dioxane for 72 h (97%). |
| | 3'-Hydroxypropiophenone Preparation Products And Raw materials |
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