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- Veratronitrile
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- $12.00
-
2026-10-16
- CAS:2024-83-1
- Min. Order: 25g
- Purity: 0.98
- Supply Ability: 25kg
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| | 2,3-Dimethoxybenzonitrile Basic information |
| | 2,3-Dimethoxybenzonitrile Chemical Properties |
| Melting point | 68-70 °C(lit.) | | Boiling point | 290.25°C (rough estimate) | | density | 1.2021 (rough estimate) | | refractive index | 1.5300 (estimate) | | Fp | >230 °F | | storage temp. | Sealed in dry,Room Temperature | | solubility | Soluble in methanol. | | form | powder to crystal | | color | White to Light yellow | | BRN | 1451651 | | InChI | 1S/C9H9NO2/c1-11-8-4-3-7(6-10)5-9(8)12-2/h3-5H,1-2H3 | | InChIKey | OSEQIDSFSBWXRE-UHFFFAOYSA-N | | SMILES | COc1ccc(cc1OC)C#N | | CAS DataBase Reference | 2024-83-1(CAS DataBase Reference) |
| Hazard Codes | Xn,T,Xi | | Risk Statements | 20/21/22-36/37/38 | | Safety Statements | 26-36 | | RIDADR | 3276 | | WGK Germany | 3 | | RTECS | DI4355000 | | HazardClass | 6.1 | | PackingGroup | III | | HS Code | 2926907090 | | Storage Class | 11 - Combustible Solids | | Hazard Classifications | Acute Tox. 4 Dermal
Acute Tox. 4 Inhalation
Acute Tox. 4 Oral
Eye Irrit. 2
Skin Irrit. 2
STOT SE 3 |
| | 2,3-Dimethoxybenzonitrile Usage And Synthesis |
| Chemical Properties | white to light yellow crystal powder | | Uses | 3,4-Dimethoxybenzonitrile is used as an organic chemical synthesis intermediate. | | Preparation | Veratraldoxime(88–89 g, 0.45 mol) was combined with acetic anhydride (100 g) in a 300-mL round-bottomed flask equipped with a ground-glass air condenser, and the mixture was cautiously heated. A vigorous reaction took place, at which point the flame (heating by oil bath; the author) was removed. After the reaction had subsided, the solution was gently refluxed for 2 h and then carefully poured, with stirring, into cold water (300 mL). Stirring was continued, and on cooling the nitrile separated as small, almost colorless crystals; these were collected by filtration and dried in air. The veratronitrile thus obtained was quite pure; yield 57–62 g (72–76%); mp 66–67 C°.
1-Cyanoacenaphthene 1403 can be synthesized from its carbaldoxime by dehydration with acetic anhydride in 87% yield. Whereas acetic anhydride usually serves as the solvent as well as the reactant, this procedure is performed in n-octane. | | Synthesis Reference(s) | Synthesis, p. 510, 1985 DOI: 10.1055/s-1985-31253 |
| | 2,3-Dimethoxybenzonitrile Preparation Products And Raw materials |
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