- 1-Propanesulfonyl chloride
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- $115.00 / 1KG
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2023-12-26
- CAS:10147-36-1
- Min. Order: 1KG
- Purity: 98% Min.
- Supply Ability: Supply according to order quantity
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| | 1-Propanesulfonyl chloride Basic information |
| | 1-Propanesulfonyl chloride Chemical Properties |
| | 1-Propanesulfonyl chloride Usage And Synthesis |
| Chemical Properties | Light yellow liquid | | Uses | 1-Propanesulfonyl chloride was used in synthesis of 1-alkyl-3-methylimidazolium alkanesulfonate ionic liquids. | | Synthesis |
2,4,6-Trichloro-[1,3,5]-triazine (TCT) was added at room temperature to a solution of propane-1-sulfonic acid in acetone dry, followed by NEt3 dropwise. The resulting mixture was irradiated to 80 °C (50 W of MW power) for 20 min in a sealed tube (10 mL pressure-rated reaction vial) in a self-tuning single-mode irradiating synthesizer. The mixture was cooled rapidly to room temperature by passing compressed air through the microwave cavity for 1 min. After cooling to room temperature, the precipitate was filtered off on Celite to afford 1-Propanesulfonyl chloride[1].
| | References | [1] Lidia De Luca, Giampaolo Giacomelli. “An Easy Microwave-Assisted Synthesis of Sulfonamides Directly from Sulfonic Acids.” The Journal of Organic Chemistry 73 10 (2008): 3967–3969. |
| | 1-Propanesulfonyl chloride Preparation Products And Raw materials |
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