- 5-Nitroanthranilonitrile
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- $1.00 / 1Kg/Bag
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2023-04-12
- CAS:17420-30-3
- Min. Order: 1Kg/Bag
- Purity: 99.66% HPLC
- Supply Ability: 5000tons/year
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| | 5-Nitroanthranilonitrile Basic information |
| | 5-Nitroanthranilonitrile Chemical Properties |
| Melting point | 200-207 °C(lit.) | | Boiling point | 290.19°C (rough estimate) | | density | 1.4141 (rough estimate) | | refractive index | 1.5500 (estimate) | | Fp | 234 °C | | storage temp. | Keep in dark place,Inert atmosphere,Room temperature | | solubility | DMSO (Slightly) | | form | Solid | | pka | -1.97±0.10(Predicted) | | color | Dark Yellow | | BRN | 1425714 | | CAS DataBase Reference | 17420-30-3(CAS DataBase Reference) | | EPA Substance Registry System | Benzonitrile, 2-amino-5-nitro- (17420-30-3) |
| Hazard Codes | Xn | | Risk Statements | 20/21/22-36/37/38 | | Safety Statements | 22-24/25-36-26 | | WGK Germany | 2 | | RTECS | BX2500000 | | TSCA | Yes | | HS Code | 29269090 | | Toxicity | mouse,LD50,oral,6710mg/kg (6710mg/kg),Gigiena Truda i Professional'nye Zabolevaniya. Labor Hygiene and Occupational Diseases. Vol. 30(1), Pg. 50, 1986. |
| | 5-Nitroanthranilonitrile Usage And Synthesis |
| Chemical Properties | yellow to brownish powder. 2-Amino-5-nitrobenzonitrile [17420-30-3], 2-cyano-4-nitroaniline, Mr 163.13, mp 210℃, is readily soluble in acetone, chloroform, and benzene; it is sparingly soluble in water and ethanol. As already mentioned, the reaction of 2-chloro5-nitrobenzonitrile with ammonia gives 2-amino-5-nitrobenzonitrile, an intermediate for azo dyes. | | Production Methods | A newer synthetic route
starts from 6-nitroisatoic anhydride [2H-3,1-benzoxazine-6-nitro-2,4 (1H)-dione]: the latter is
converted into 2-amino-5-nitrobenzonitrile by
reaction with ammonia, subsequent treatment
with phosgene in dimethylformamide or Nmethylpyrrolidone, followed by hydrolysis of
the formamidine.
 | | Synthesis Reference(s) | Journal of the American Chemical Society, 82, p. 3152, 1960 DOI: 10.1021/ja01497a043 |
| | 5-Nitroanthranilonitrile Preparation Products And Raw materials |
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