Chloromethyl Trimethylsilyl Ether

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Chloromethyl Trimethylsilyl Ether Basic information
Product Name:Chloromethyl Trimethylsilyl Ether
Synonyms:Chloromethyl Trimethylsilyl Ether;(Chloromethoxy)trimethylsilane;Silane, (chloromethoxy)trimethyl-
CAS:23586-77-8
MF:C4H11ClOSi
MW:138.67
EINECS:
Product Categories:
Mol File:23586-77-8.mol
Chloromethyl Trimethylsilyl Ether Structure
Chloromethyl Trimethylsilyl Ether Chemical Properties
solubility sol dichloromethane
Safety Information
MSDS Information
Chloromethyl Trimethylsilyl Ether Usage And Synthesis
PreparationChloromethyl Trimethylsilyl Ether is prepared in situ under nitrogen by addition of a cooled (-78 °C) solution of Sulfuryl Chloride (1 equiv) in dry dichloromethane (2 M) to a solution of ethyl (trimethylsilyloxy)methyl sulfide in dichloromethane (1 M)[1].
storageChloromethyl Trimethylsilyl Ether is low stability; best prepared in situ at low temperature.
References1. Gundersen, L.-L.; Benneche, T. ACS 1991, 45, 975.
Chloromethyl Trimethylsilyl Ether Preparation Products And Raw materials
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